Fritsch Vibratory Micro Mill PULVERISETTE 0 Operating instructions

Brand: Fritsch

Model: Vibratory Micro Mill PULVERISETTE 0

Type: Operating instructions

Operang

instrucons

VIBRATORY MICRO MILL

PULVERISETTE 0

Read the instrucons prior to performing any task!

Valid starng with: 00.6020/0215

Translaon of the original operang instrucons

Version 04/2022 Index 010

Fritsch GmbH

Milling and Sizing

Industriestraße 8

D - 55743 Idar-Oberstein

Telephone: +49 6784 70-0

Email: inf[email protected]

Internet: www.fritsch.de

Cercaons and CE conformity

Cercaon

CE Conformity

Cercaons and CE conformity

Fritsch GmbH has been cered by the SGS-TÜV Saar GmbH.

An audit cered that Fritsch GmbH conforms to the requirements of the DIN EN

ISO 9001:2015.

The enclosed Conformity Declaraon lists the guidelines the FRITSCH instrument

conforms to, to be able to bear the CE mark and the UKCA mark!

Table of contents

1 Basic structure. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

2Safety informaon and use. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

2.1 Requirements for the user. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

2.2 Scope of applicaon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

2.2.1 Operang principle. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

2.2.2 Amplitude control. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

2.3 Obligaons of the operator. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

2.4 Informaon on hazards and symbols used in this manual. . . . . . . . . . . . 9

2.5 Device safety informaon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

2.6 Protecve equipment. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

2.7 Hazardous points. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

2.8 Electrical safety. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

2.8.1 General informaon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

2.8.2 Protecon against restart. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

2.8.3 Overload protecon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

3Technical data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

3.1 Dimensions. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

3.2 Weight. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

3.3 Operang noise. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

3.4 Voltage. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

3.5 Current consumpon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

3.6 Protecon class. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

3.7 Power consumpon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

3.8 Electrical fuses. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

3.9 Load. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

3.10 Material. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

3.11 Final neness of a grinding process with the PULVERISETTE 0. . . . . . . . . 15

4Installaon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

4.1 Transport. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

4.2 Unpacking. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

4.3 Seng up. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

4.4 Ambient condions. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

4.5 Electrical connecon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

4.5.1 Adjusng the mains voltage. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

Table of contents

5Inial start-up. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19

5.1 Switching on. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19

5.2 Funcon check. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19

5.3 Switching o. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19

6 Using the device. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20

6.1 Conducng a grinding operaon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20

6.1.1 Parameters. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20

6.1.2 Fing and clamping the mortar. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20

6.1.3 Grinding with liquid nitrogen. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21

6.2 Seng the grinding duraon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22

6.3 Seng the amplitude. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23

6.3.1 Displaying the amplitude. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23

7Accessories. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24

7.1 Sound absorpon hood. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24

7.2 Conversion to Vibratory Sieve Shaker ANALYSETTE 3 SPARTAN. . . . . . . . 24

7.2.1 Conducng a sieve analysis. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24

7.2.2 Dry sieving. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27

7.2.3 Wet sieving. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27

7.2.4 Cleaning the test sieves (mesh wire sieves). . . . . . . . . . . . . . . . . . . . . . 29

7.2.5 Seng the sieving me. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30

7.2.6 Seng and displaying the amplitude. . . . . . . . . . . . . . . . . . . . . . . . . . . 30

7.2.7 TorqueMaster for easy clamping of the sieve set. . . . . . . . . . . . . . . . . 31

8 Cleaning. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35

8.1 Cleaning the device. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35

8.2 Cleaning grinding elements. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35

9Maintenance. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36

10 Repairs. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37

10.1 Checklist for troubleshoong. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37

11 Disposal. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38

12 Guarantee terms. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39

13 Exclusion of liability. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41

14 Safety logbook. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43

15 Index. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46

Basic structure

1 Basic structure

The PULVERISETTE 0 is equivalent in design to the ANALYSETTE

3 SPARTAN, except that the ANALYSETTE 3 SPARTAN, like the

PRO version, also uses a sieve set.

1 Lid (also used in the ANALYSETTE 3 as a clamping lid for the

100 mm test sieves)

2 Mortar with grinding ball

3 Vibratory plate

4 Knurled knob

5 Toothed belt

6 Belt clamping device

7 Control panel

Safety informaon and use

2 Safety informaon and use

2.1 Requirements for the user

This operang manual is intended for persons assigned with operang and moni-

toring the Fritsch of the PULVERISETTE 0. The operang manual and especially

its safety instrucons are to be observed by all persons working on or with this

device. In addion, the applicable rules and regulaons for accident prevenon

at the installaon site are to be observed. Always keep the operang manual at

the installaon site of the of the PULVERISETTE 0.

People with health problems or under the inuence of medicaon, drugs, alcohol

or exhauson must not operate this device.

The of the PULVERISETTE 0 may only be operated by authorised persons and

serviced or repaired by trained specialists. All commissioning, maintenance and

repair work may only be carried out by technically qualied personnel. Qualied

personnel are persons who, because of their educaon, experience and training

as well as their knowledge of relevant standards, regulaons, accident prevenon

guidelines and operang condions, are authorised by those responsible for the

safety of the machine to carry out the required work and are able to recognize

and avoid possible hazards as dened for skilled workers in IEC 364.

In order to prevent hazards to users, follow the instrucons in this manual.

Malfuncons that impair the safety of persons, the of the PULVERISETTE 0 or

other material property must be reced immediately. The following informaon

serves both the personal safety of operang personnel as well as the safety of

the products described and any devices connected to them: All maintenance and

repair work may only be performed by technically qualied personnel.

This operang manual is not a complete technical descripon. Only the details

required for operaon and maintaining usability are described.

Fritsch has prepared and reviewed this operang manual with the greatest care.

However, no guarantee is made for its completeness or accuracy.

Subject to technical modicaons.

2.2 Scope of applicaon

NOTICE

This laboratory instrument is designed for an 8-hour shi oper-

aon at 30 % duty cycle and not for connuous operaon.

The duty cycle is dened as the rao of load duraon to run

me. The run me is dened as load duraon plus pause me.

According to DIN EN 60034-1 (VDE 0530, IEC34-1) a connuous

operaon already takes place aer a standardised run me of

10 minutes. At 30 % duty cycle (DC = rao of load duraon to

run me) a load duraon of 3 minutes and a pause me of 7

minutes would be within standard.

If the standardised run me of 10 minutes is exceeded, then,

by denion, there would be a connuous operaon and

disproporonate temperature increases may occur, possibly

involving increased wear.

Safety informaon and use

The "Vibratory Micro Mill PULVERISETTE 0" is used for the ne comminuon

of dry laboratory sample material or suspensions. It is used for homogenising

emulsions or pastes.

2.2.1 Operang principle

The plasc housing contains a solid cast structure with an electronically con-

trolled electromagnet. Three permanently exible at springs carry the pole plate

of this magnet together with the vibratory plate, which is fastened to it. When

the magnet is switched on, the pole plate and vibratory plate are aracted and

spring back when it is switched o. The cast structure and magnet on one side

and the pole plate, vibratory plate and sieves on the other side form a vibratory

system.

The dierent weights of the mortar material or grinding balls change the natural

frequency of the vibratory system. For this reason, it is not always possible to

set the amplitude of the micro mill opmally e.g. with a constant 50 Hz mains

frequency present. The processor-controlled electronics of the PULVERISETTE 0

micro mill ensure a precisely adjustable, reproducible oscillaon amplitude. This

is achieved by bringing the frequency to smulate oscillaon closer to the natural

frequency of the system or farther away from it. The desired oscillaon ampli-

tude of the grinding set between 0.1 mm and 3.0 mm can always be achieved -

and with relavely low energy input. Therefore, connuous operaon is possible

without heang the sample material and the overall mill system.

The mortar bowl with 50 mm diameter grinding ball (or 70 mm for agate only)

and grinding stock oscillates vercally. This causes the grinding ball in the mortar

bowl to vibrate and comminute the grinding stock by impact and fricon.

2.2.2 Amplitude control

An electronic control circuit guides the oscillaon frequency of the PULVERISETTE

0 from a high to a low frequency range. In the meanme, a measuring system

records the amplitude and reports it to the control circuit unl the preselected

amplitude is reached.

This amplitude control takes place at regular intervals during the enre opera-

on. This makes it possible to react to changes in the vibratory system.

The amplitude of the PULVERISETTE 0 is set manually with the Plus and Minus

key on the control panel and viewed on the lid.

2.3 Obligaons of the operator

Before using the of the PULVERISETTE 0, this manual is to be carefully read and

understood. The use of the of the PULVERISETTE 0 requires technical knowledge;

only commercial use is permied.

The operang personnel must be familiar with the content of the operang

manual. For this reason, it is very important that these persons actually receive

the present operang manual. Ensure that the operang manual is always near

the device.

The of the PULVERISETTE 0 may exclusively be used within the scope of appli-

caons set down in this manual and within the framework of guidelines put

forth in this manual. In case of non-compliance or improper use, the customer

assumes full liability for the funconal capability of the PULVERISETTE 0 and for

any damage or injury arising from failure to full this obligaon.

Safety informaon and use

Safety informaon

By using the of the PULVERISETTE 0 the customer agrees with this and recognizes

that defects, malfuncons or errors cannot be completely excluded. To prevent

risk of damage to persons or property or of other direct or indirect damage,

resulng from this or other causes, the customer must implement sucient and

comprehensive safety measures for working with the of the PULVERISETTE 0.

Neither compliance with this manual nor the condions and methods used

during installaon, operaon, use and maintenance of the of the PULVERISETTE

0 can be monitored by Fritsch GmbH. Improper execuon of the installaon can

result in property damage and thus endanger persons. Therefore, we assume

absolutely no responsibility or liability for loss, damage or costs that result from

errors at installaon, improper operaon or improper use or improper mainte-

nance or are in any way connected to these.

The applicable accident prevenon guidelines must be complied with.

Generally applicable legal and other obligatory regulaons regarding environ-

mental protecon must be observed.

2.4 Informaon on hazards and symbols used in this manual

Safety informaon in this manual is designated by symbols. Safety informaon is

introduced by keywords that express the extent of the hazard.

DANGER

This symbol and keyword combinaon points out a directly

hazardous situaon that can result in death or serious injury if

not avoided.

WARNING

This symbol and keyword combinaon points out a possibly

hazardous situaon that can result in death or serious injury if

not avoided.

CAUTION

This symbol and keyword combinaon points out a possibly

hazardous situaon that can result in slight or minor injury if

not avoided.

NOTICE

This symbol and keyword combinaon points out a possibly

hazardous situaon that can result in property damage if not

avoided.

ENVIRONMENT

This symbol and keyword combinaon points out a possibly

hazardous situaon that can result in environmental damage if

not avoided.

Special safety informaon

To call aenon to specic hazards, the following symbols are used in the safety

informaon:

Safety informaon and use

DANGER

This symbol and keyword combinaon points out a directly haz-

ardous situaon due to electrical current. Ignoring informaon

with this designaon will result in serious or fatal injury.

DANGER

This symbol and keyword combinaon designates contents and

instrucons for proper use of the machine in explosive areas

or with explosive substances. Ignoring informaon with this

designaon will result in serious or fatal injury.

DANGER

This symbol and keyword combinaon designates contents

and instrucons for proper use of the machine with combus-

ble substances. Ignoring informaon with this designaon will

result in serious or fatal injury.

WARNING

This symbol and keyword combinaon points out a directly

hazardous situaon due to movable parts. Ignoring informaon

with this designaon can result in hand injuries.

WARNING

This symbol and keyword combinaon points out a directly

hazardous situaon due to hot surfaces. Ignoring informaon

with this designaon can result in serious burn injuries due to

skin contact with hot surfaces.

Safety informaon in the procedure instrucons

Safety informaon can refer to specic, individual procedure instrucons. Such

safety informaon is embedded in the procedure instrucons so that the text can

be read without interrupon as the procedure is being carried out. The keywords

described above are used.

Example:

1. Loosen screw.

2. CAUTION

Risk of entrapment at the lid.

Close the lid carefully.

3. Tighten screw.

Tips and recommendaons

Safety informaon and use

Please observe!

This symbol emphasises useful ps and recommendaons as

wells as informaon for ecient operaon without malfunc-

on.

Further designaons

To emphasise procedure instrucons, results, lists, references and other ele-

ments, the following designaons are used in this manual:

Designaon Explanaon

1., 2., 3. ...

Step-by-step procedure instrucons

ðResults of steps in the procedure

References to secons in this manual and relevant

documentaon

Lists without a specic order

[Buon]

Operang elements (e.g. push buon, switch), dis-

play elements (e.g. signal lamps)

‘Display’

Screen elements (e.g. buons, funcon key assign-

ment)

2.5 Device safety informaon

■Only use original accessories and original spare parts. Failure to observe this

instrucon can compromise the safety of the machine.

■Accident-proof conduct is to be strictly followed during all work.

■Comply with all currently applicable naonal and internaonal accident pre-

venon guidelines.

CAUTION

Wear hearing protecon!

If a noise level of 85 dB(A) is reached or exceeded, ear protec-

on should be worn to prevent hearing damage.

WARNING

The maximum accepted concentraon (MAC) levels of the rel-

evant safety guidelines must be observed; if necessary, venla‐

on must be provided or the machine must be operated under

an extractor hood.

Safety informaon and use

DANGER

Explosion hazard!

−When Grinding oxidizable substances, e.g. metals or coal,

there is a risk of spontaneous combuson (dust explosion)

if the share of ne parcles exceeds a certain percentage.

When Grinding these kinds of substances, special safety

measures must be taken and the work must be supervised

from a specialist.

−The high-speed rotor mill is not explosion protected and is

not designed to grind explosive materials.

■Do not remove the informaon signs.

NOTICE

Immediately replace damaged or illegible informaon signs.

■Unauthorised alteraon of the of the PULVERISETTE 0 will void Fritsch's

declaraon of conformity to European direcves and void the guarantee.

■Only use the of the PULVERISETTE 0 when it is in proper working order,

as intended and in a safety- and hazard-conscious manner adhering to the

operang manual. In parcular, immediately recfy any malfuncons that

could pose a safety hazard.

■If, aer reading the operang manual, there are sll quesons or problems,

please do not hesitate to contact our specialised personnel.

2.6 Protecve equipment

Protecve equipment is to be used as intended and may not

be disabled or removed.

All protecve equipment is to be regularly checked for integ-

rity and proper funconing.

NOTICE

−The toothed belts must only be released or clamped in the

switched o state.

−Before switching on again, ensure that the two toothed

belts are evenly, ghtly clamped using the knurled knobs.

2.7 Hazardous points

■Crushing hazard at the mortar clamping device

■Crushing hazard between vibratory plate and housing

Safety informaon and use

2.8 Electrical safety

2.8.1 General informaon

The main switch separates the device from the mains on two poles.

2.8.2 Protecon against restart

Aer switching o at the main switch and switching on again, the START key must

be pressed for start-up.

2.8.3 Overload protecon

The mains fuse provides overload protecon.

Technical data

3 Technical data

3.1 Dimensions

Without grinding set:

350 x 200 x 400 mm (width x height x depth)

3.2 Weight

Net: 21 kg

Gross: approx. 27 kg

3.3 Operang noise

Emissions value of workplace according to DIN EN ISO 3746:2005 is up to 76.6

dB (A) for grinding gravel. The value uctuates depending on frequency, grinding

stock and the material of the grinding set.

When grinding with the PULVERISETTE 0, the operang noise is greatly reduced

by using the sound absorpon hood made of plexiglas (order no.: 00.0130.17).

3.4 Voltage

The device can be operated in two voltage ranges:

■Single phase alternang current 115V ± 10% and

■Single phase alternang current 230 V ± 10%.

(See also ⮫

Chapter 4.5 ‘Electrical connecon’ on page 17

)

It is not necessary to change the voltage range manually.

3.5 Current consumpon

Depending on the mains voltage, the maximum current consumpon is in the

ranges:

■115 V ® 0.44 A

■230 V ® 0.22 A

3.6 Protecon class

IP 22

3.7 Power consumpon

Depending on the voltage range, the maximum power consumpon is approx. 50

3.8 Electrical fuses

■Fuse under mains switch (on the back of the device)

Replacement: 4 A M micro fuse, 5 x 20 mm

Technical data

3.9 Load

The maximum load of the PULVERISETTE 0 is up to 6 kg!

3.10 Material

■Maximum feed size 5 mm

■Maximum feed quanty 10 ml

3.11 Final neness of a grinding process with the PULVERISETTE 0

The achievable nal neness (PULVERISETTE 0) of the grinding stock is approx. 10

µm. (Depending on the grindability of the sample and the grinding duraon)

Installaon

4Installaon

4.1 Transport

The device is delivered in a cardboard box. In the case of delivery with several

accessories, the device is delivered in a transport crate.

WARNING

Improper liing can lead to personal injury or property

damage. The machine must only be lied with suitable equip-

ment by qualied personnel.

The guarantee excludes all claims for damage due to improper transport.

4.2 Unpacking

■In the case of delivery in a crate, pull out the nails that fasten the lid to the

surrounding packaging.

■Remove the lid.

■Take out the accessories.

■To remove the device, three hexagon screws under the wooden plate must

be unscrewed.

■Compare the contents of the delivery with your order.

Keep the wooden plate, screws and washers, as this transport

securing device must be reaached in the case of further

transport or return.

4.3 Seng up

NOTICE

Allow the device to acclimase for two hours before commis-

sioning. High temperature dierences can lead to condensaon

in the device and damage to the electronics aer switching on.

Strong temperature uctuaons can occur during transport or interim storage.

Depending on the temperature dierence between the installaon site and the

transport or storage environment, condensaon can form inside the device. This

can damage the electronics if the devices are switched on too early. Wait for at

least two hours aer setup before switching on the device.

■Place the device on a at, stable surface. It does not have to be fastened to

the surface. Leave sucient space beside the device for placing the accesso-

ries used.

■The space behind the device must be freely accessible so that the main

switch on the mains connecon can be accessed quickly in case of emer-

gency.

■The device rests on three at coil spring assemblies. Level the micro mill:

Installaon

–PULVERISETTE 0:

Level the micro mill by screwing these feet in or out so that during

grinding, the grinding stock is evenly distributed on the walls of the

mortar bowl.

4.4 Ambient condions

WARNING

Mains voltage!

−The device may only be operated indoors.

−The surrounding air may not carry any electrically conduc-

ve dust.

−Maximum relave humidity 80% for temperatures up to

31°C, linearly decreasing down to 50% relave humidity at

40°C.

■The room temperature has to stay between 5 - 40°C.

■Altudes up to 2000 m

■Degree of polluon 2 according to IEC 664.

4.5 Electrical connecon

Before establishing the connecon, compare the voltage and current values

stated on the type plate with the values of the mains system to be used.

CAUTION

Ignoring the values on the type plate may result in damage to

the electrical and mechanical components.

4.5.1 Adjusng the mains voltage

CAUTION

If the value 01 is set at a voltage of 230V~, it will result in a

defect in the sieve shaker during operaon. Failure to observe

this will render void the guarantee, and releases us from lia-

bility for any resulng damage to the device.

NOTICE

Only qualied personnel may change the voltage range on the

device!

1. Switch main switch to "0".

2. Switch the device on at the main switch while holding down the Stop key.

The device is now in "Setup" mode.

3. The "Sieving Time" display now shows the default seng "02" for 230 V,

"01" for 115 V.

Installaon

4. These values can be changed with the "Sieving Time" +/- key and adapted

to the mains voltage.

■230 V - 02

■115 V - 01

Save the set values by clicking the stop key.

5. Aer making adjustments, switch on the main switch again.

Inial start-up

5Inial start-up

Perform inial start-up only aer all work as described in ⮫

Chapter 4 ‘Installa-

on’ on page 16

has been carried out.

5.1 Switching on

■The device must be connected to the power supply if this has not been done

already.

■Switch on the device with the main switch on the back of the device.

■The POWER lamp on the control panel lights up.

■The display shows the default seng.

5.2 Funcon check

■Fill the mortar (2) with 5 - 10 ml of sand, insert the grinding ball and clamp

the lid (1).

■Set the amplitude to 2 mm (See ⮫

Chapter 6.3 ‘Seng the amplitude’

on page 23

)

■When everything is correctly clamped, start the funcon check with "START".

Whether the set amplitude has been reached can be checked

on the display or on the amplitude plate on the lid.

5.3 Switching o

■Press the STOP key and switch o the main switch.

Using the device

6 Using the device

NOTICE

Please note that when using the grinding set made of agate,

that the agate is a natural stone. This means that its hardness

and consistency may vary. In transion areas of the Mohs hard-

ness of your sample material, the agate grinding set can show

great wear or even breaking characteriscs, depending on the

degree of the load.

In such cases, check the grinding set regularly during the

grinding to avoid irreversible damage.

6.1 Conducng a grinding operaon

6.1.1 Parameters

Grinding duraon 10 ... 30 min (average)

Amplitude 1 ... 2 mm (max.)

Feed quanty Max. 10 ml (parcle feed size ≤ 5

mm)

6.1.2 Fing and clamping the mortar

1. Move the clamping lever on the belt clamping device downwards and

insert the toothed belt through the holder from the inside to the outside.

2. Place the mortar and the ball on the vibratory plate. The mortar must be

posioned in the round gap of the vibratory plate without being wedged.

3. Unscrew the knurled knob on the toothed belt as far as possible.

4. Pour in the grinding stock.

5. Put on the clamping lid.

6. Aach the knurled knob to the lid

7. Lightly pull the toothed belt ght and move it upwards unl its teeth

interlock with the teeth of the belt clamping device.

8. Move the clamping lever upwards.

Make sure that the teeth of the toothed belt interlock

with the teeth of the belt clamping device!

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Fritsch Vibratory Micro Mill PULVERISETTE 0 Operating instructions

Fritsch Vibratory Micro Mill PULVERISETTE 0 Operating instructions

Fritsch Vibratory Micro Mill PULVERISETTE 0 Operating instructions

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