Mettler Toledo InPro 6000 Amperometric O2 Sensors Operating instructions

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6 InPro 6000 Aperometric O
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Sensors
© 06 / 2019Mettler-ToledoGmbH AmperometricSensorSeries
30 313 395 B PrintedinSwitzerland
6.1 Doplňování elektrolytu, výměna korpusumembrány
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6.1 Genopfyldning af elektrolyt;
udskiftning af membrandelen
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6.1 Nachfüllen von Elektrolyten; Austausch des
Membrankörpers
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1 Introduction ................................................................... 21
2 Safetyinstructions .......................................................... 21
3 Productdescription ........................................................ 21
4 Installation .................................................................... 22
4.1 Connection .................................................................... 22
4.2 Mountingthesensor ....................................................... 22
5 Operation ..................................................................... 23
5.1 Start-upandpolarizing ................................................... 23
5.2 Calibration .................................................................... 23
6 Maintenance .................................................................. 23
6.1 Rellingelectrolyte;exchangingmembranebody ............... 24
7 Disposal ....................................................................... 25
8 Warranty ....................................................................... 25
9 Storageconditions ......................................................... 25
10 ECDeclarationofConformity ........................................... 25
Contents
InPro 6000
Amperometric O
2
Sensors
Quick Setup Guide
InProandISMareregisteredtrademarksof
Mettler-ToledoGmbHinSwitzerland,theUSA,
theEuropeanUnionandafurthervecountries.
en
Appendix
TechnicalDrawings ..................................................................110
en QuickSetupGuide
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1 Introduction
Thankyouforbuyingthisamperometricoxygensensorfrom
METTLERTOLEDO.TheInPro6000(i)seriesamperometric
O
2
sensors are intendedsolely for in-line measurement
oftheoxygenpartialpressuree.g.,oxygenmeasurement
inliquids.
Applicationexamplesare(butnotlimitedto),fermentation
in biotechnology, oxygen measurement in brewing and
chemicalapplications.
The followingsensor types arecoveredwithinthisquick
set-upguide.
InPro6800/InPro6850i/InPro6900/InPro6900i/
InPro6950/InPro6950i/easySense.
Sensorswithout’i’areanalogsensorsandwith’i’aredigital
sensorsincorporatingIntelligentSensorManagement(ISM).
EasySenseisdigitalsensorwithoutISM.ISMfunctionality
offerPlugandMeasure as well asenhanceddiagnostics
features.
2 Safety instructions
h
Notice:Beforeeverystart-up,thesensormustbechecked
for:
–Damagetotheconnections,fastenings,etc.
–Leakage
–Perfectfunctioning
–Authorization for use in conjunction with other plant
equipmentandresources.
h
Notice:Themanufacturer/supplieracceptsnoresponsibility
for any damage caused by unauthorized attachments
or for the incorporation of spare parts which are not of
METTLERTOLEDOprovenance.Theriskisborneentirelyby
theoperator.
a
Caution:Beforethesensorisputintooperation,the
operatormusthavealreadyclariedthatuseofthesensor
in conjunction with the other associated equipment and
resourcesisfullyauthorized.
a
Caution:A defectivesensormay neitherbeinstallednor
putintooperation.Faultycontainmentorinstallationoutof
conformancewithregulationsandinstructionscanleadto
theescapeofmediumortopressuresurges(explosion),
potentiallyharmfulbothtopersonsandtotheenvironment.
a
Caution: Thesensorisnotequippedwithheatprotection.
Duringsteam-sterilizationproceduresinpipes,thesurface
ofthesensorcanreachhightemperaturesandcauseburns.
a
Caution: Somecomponentsinsidethesensorareenergized
withvoltages which can cause lethal shocksin case of
contact. The instrument needs to be switched to zero
potentialbeforeanyoperationonthewiringterminal.
a
Warning: Beforedismantlingthesensororcommencingany
maintenanceworkonit,ensurethattheequipmentinwhich
thesensorisinstalledisinasafecondition(pressurize,
noexplosionrisk,empty,rinse,vent,etc.).
3 Product description
h
Notice:Digitalsensors(ISM):Allsensorsendingwithan’i’
aredelivereddryandmustbelledwithelectrolytebefore
start-up.Electrolyte has to be ordered separately.
Analogsensorsaredeliveredlledwithelectrolyte,however,
itisadvisedtoreplacetheelectrolytereservoirwithfresh
solution.
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Article Nr.: Electrolytes
59907065–O
2
Electrolyte25mL(InPro6050;
InPro6800;InPro6850i;easySense)
52206107–O
2
Electrolyte25mLHighSalinity
[InPro6900(i);InPro6950(i)]
30298424–O
2
electrolytepack3×25mL
(InPro6050;InPro6800;InPro6850i;
easySense)
30298425–O
2
electrolytepack–highsalinity3×25mL
[InPro6900(i);InPro6950(i)]
a
Warning: The O
2
electrolytehasanalkalinepHvalue.
Contactofelectrolytewithmucousmembraneoreyesis
to be avoided. Therefore protective gloves and safety
glasses have to be worn for the following dismantling
works.Ifsuchcontactoccurs,theaffectedareashouldbe
wellrinsedwithwater.Inthecaseofaccident,orshouldever
anyadversesignsappear,getimmediatemedicalattention.
4 Installation
4.1 Connection
The sensors are installed to a transmitter by using a VP
(analogsensors) or AK9 (ISMsensors) connector cable.
Cables in different lengths 2–50 m are available from
METTLERTOLEDO.
h
Notice:Cableand terminal assignment can be foundin
theMETTLERTOLEDOcableand/ortransmitterinstruction
manual.
VPconnector Slit Pin Plug VP-6cable
K8S(ISM) AK9(ISM)
O
2
Transmitter VPorAK9cable
4.2 Mounting the sensor
Before mounting the sensor into a housing remove the
protectioncaponthesensor.Thesensorcanthenbemounted
intoanInFit/InTracSerieshousingfromMETTLERTOELDO.
Alternatively,the12mmsensorscan bemounteddirectly
throughasocketwithinsidethreadPg13.5andsecurely
tightenedviathePg13.5threadedsleeve.
h
Notice:Forconnecting the cable tothe terminals ofthe
transmitter, please refer to the instructions given in the
METTLERTOLEDOtransmittermanual(www.mt.com/pro-
transmitters)
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5 Operation
5.1 Start-up and polarizing
Whenthesystemisoperatedforthersttimeorifthesensor
hasbeendisconnectedfromthevoltagesource(transmitter
or O
2
sensormaster)forlongerthan5minutes,thesensor
hastobepolarizedpriortocalibrationbyconnectingittothe
operatingO
2
transmitterortoasensormaster.After6hours,
thesensorwillbefullypolarizedandreadyforoperation.
For polarizing and storage the cleaning and conditioning
solution (order Nr. 52 200 255) is recommended. This
solutioncontainsanoxygenscavengerwhichensuresthat
theelectrolyteofthesensordoesnotcomeintocontactwith
oxygenwhennotinuse.
h
Attention:TheInPro6950ishouldneverbepolarizedatair!
It is recommended to store the sensors in the according
electrolyteorcleaningandconditioningsolutionduringthe
polarizationtime.TheInPro6900iand6950iuseaspecial
electrolytewhichcontainsanoxygenscavenger.
a
Warning: Setting of the polarization voltage on the
transmitter for correct measurements:
Standardapplications:–675mV.
Measurementsofcontinuouslylowestoxygenconcentrations
(<500ppb in liquids or<10,000 ppm [vol.] ingases)
andInpresenceofvolatileacidiccomponents(e.g.carbon
dioxideduringmeasurementsinbreweries):–500mV.
5.2 Calibration
WithdigitalISMsensorsallcalibrationdataarestoredinthe
sensor.Oncelledwithelectrolyteandpolarizedtheycanbe
connectedtoanISMtransmitterandimmediatelyusedfor
measurement.Analogsensorsaredeliveredwetandafter
polarizationcanbeslope1-pt,2pt-orprocesscalibrated
usingatransmitter.
With ISM sensors METTLER TOLEDO’s calibration
and maintenance software tools iSense/iSense light
are recommended for sensor checking and calibration.
(www.mt.com/iSense).
Polarizationvoltageforcalibrationpurposesarealwaysput
to–675mV.
Formeasurements incarbondioxidecontainingsolutions
the transmitter setting has to be switched to –500 mV
accordinglyafterthecalibration.
6 Maintenance
Ifthemembraneand/ortheinteriorbodyexhibitssignsof
failure(longresponsetime,increasedcurrentinanoxygen-
freemedium,mechanicaldamage,etc.)themembranebody
and/ortheinteriorbodyhastobereplaced.
The incorporated Intelligent Sensor Management (ISM)
technologymonitorsandreportstheremaininglifetimeof
theinnerbodiesastheDynamicLifetimeIndicator.
Dependingontheaggressiveness(CIP/SIP)oftheapplication
conditionsareplacementofelectrolyte,themembranebody
or the interior body is recommended. This maintenance
can be performed by using the transmitter’s calibration
menu and/or using METTLER TOLEDO’s calibration and
maintenancetooliSense(www.mt.com/iSense).
Fordetailedmaintenancedescriptionandcriteriapleaserefer
toiSenseorthemainsensormanual.
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6.1 Relling electrolyte; exchanging membrane body
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Procedure
Cleanse with demin water; turn cap sleeve twice, do not
unmountyet.Fromthebottompushthemembranebodyout
byaslightupwardspush;unscrewcompletely.Removecap
sleeveandmembranebody.Cleaninnerbody.Ifnescessary
use new membrane body and ll with fresh electrolyte
solution. Make sure no air bubbles are trapped. Replace
O-ringeachtimewhenreplacingthemembranebodyand
screwthecapsleeveoncarefully.
7 Disposal
Itistheusersresponsibilitytodisposeofspentspareparts
and if necessary the sensor in a professional manner.
Sensorscontainelectroniccomponentsthatrequirespecial
disposalwithoutanyhazardforhumans,andwithnoriskof
harmtotheenvironment.Pleaseobservetheapplicablelocal
ornational regulations concerning thedisposal of “waste
electricalandelectronicequipment”.
8 Warranty
Onmanufacturingdefects,12monthsafterdelivery.
9 Storage conditions
Inspect the sensor immediately after receiving for any
transportdamage.Thesensorshouldbe stored in a dry,
cleanandprotectedareauntilthetimeofinstallation.Ifthe
sensorhasbeenremovedfromthe process, it should be
thoroughlycleanedanddried.Itshouldbestoredinadry,
cleanandprotectedareauntiltimeofinstallation.
10 EC Declaration of Conformity
Thecompletedeclarationisavailableinthedeclarationof
conformitycerticate.
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6.1 Rellenado de electrolito; sustitución del cuerpo
demembrana
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6.1 Elektrolyytin täyttö; kalvon rungon vaihto
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© 06 / 2019Mettler-ToledoGmbH AmperometricSensorSeries
30 313 395 B PrintedinSwitzerland
6.1 Remplissage d’électrolyte;
remplacement ducorps à membrane
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48 InPro 6000 Aperometric O
2
Sensors
© 06 / 2019Mettler-ToledoGmbH AmperometricSensorSeries
30 313 395 B PrintedinSwitzerland
6.1 Az elektrolit feltöltése, a membrántest cseréje
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hu
54 InPro 6000 Aperometric O
2
Sensors
© 06 / 2019Mettler-ToledoGmbH AmperometricSensorSeries
30 313 395 B PrintedinSwitzerland
6.1 Ricarica dell’elettrolita; sostituzione del corpo
della membrana
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60 InPro 6000 Aperometric O
2
Sensors
© 06 / 2019Mettler-ToledoGmbH AmperometricSensorSeries
30 313 395 B PrintedinSwitzerland
6.1
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ja
66 InPro 6000 Aperometric O
2
Sensors
© 06 / 2019Mettler-ToledoGmbH AmperometricSensorSeries
30 313 395 B PrintedinSwitzerland
6.1 전해질 재충진; 멤브레인 본체 교환
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ko
68 InPro 6000 Aperometric O
2
Sensors
© 06 / 2019Mettler-ToledoGmbH AmperometricSensorSeries
30 313 395 B PrintedinSwitzerland
1 Inleiding ........................................................................ 69
2 Veiligheidsinstructies ...................................................... 69
3 Productbeschrijving ........................................................ 69
4 Installatie ...................................................................... 70
4.1 Aansluiting .................................................................... 70
4.2 Desensormonteren ....................................................... 70
5 Bediening ..................................................................... 71
5.1 Opstartenenpolariseren ................................................. 71
5.2 Kalibratie ...................................................................... 71
6 Onderhoud .................................................................... 71
6.1 Bijvullingelektrolyt;vervangingmembraanlichaam ............ 72
7 Afvoeren ........................................................................ 73
8 Garantie ........................................................................ 73
9 Opslagomstandigheden .................................................. 73
10 EG-verklaringvanovereenstemming ................................ 73
Inhoud
InPro 6000
Amperometrische O
2
-sensoren
Beknopte handleiding
InProenISMzngedeponeerdehandelsmerken
vanMettler-ToledoGmbHinZwitserland,deVS,
deEuropeseUnieenvfanderelanden.
nl
Blage
Technischetekeningen .............................................................. 110
nl Beknoptehandleiding
72 InPro 6000 Aperometric O
2
Sensors
© 06 / 2019Mettler-ToledoGmbH AmperometricSensorSeries
30 313 395 B PrintedinSwitzerland
6.1 Bvulling elektrolyt; vervanging membraanlichaam
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nl
78 InPro 6000 Aperometric O
2
Sensors
© 06 / 2019Mettler-ToledoGmbH AmperometricSensorSeries
30 313 395 B PrintedinSwitzerland
6.1 Uzupełnianie elektrolitu; wymiana korpusu
membrany
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pl
84 InPro 6000 Aperometric O
2
Sensors
© 06 / 2019Mettler-ToledoGmbH AmperometricSensorSeries
30 313 395 B PrintedinSwitzerland
6.1 Relamento de eletrólito;
troca do corpo demembrana
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pt
/