Mettler Toledo InPro 6000 Amperometric O2 Sensors Operating instructions

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6.1 Doplňování elektrolytu, výměna korpusumembrány

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6.1 Genopfyldning af elektrolyt;

udskiftning af membrandelen

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6.1 Nachfüllen von Elektrolyten; Austausch des

Membrankörpers

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1 Introduction ................................................................... 21

2 Safetyinstructions .......................................................... 21

3 Productdescription ........................................................ 21

4 Installation .................................................................... 22

4.1 Connection .................................................................... 22

4.2 Mountingthesensor ....................................................... 22

5 Operation ..................................................................... 23

5.1 Start-upandpolarizing ................................................... 23

5.2 Calibration .................................................................... 23

6 Maintenance .................................................................. 23

6.1 Rellingelectrolyte;exchangingmembranebody ............... 24

7 Disposal ....................................................................... 25

8 Warranty ....................................................................... 25

9 Storageconditions ......................................................... 25

10 ECDeclarationofConformity ........................................... 25

Contents

InPro 6000

Amperometric O

2

Sensors

Quick Setup Guide

InProandISMareregisteredtrademarksof

Mettler-ToledoGmbHinSwitzerland,theUSA,

theEuropeanUnionandafurthervecountries.

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Appendix

TechnicalDrawings ..................................................................110

en QuickSetupGuide

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1 Introduction

Thankyouforbuyingthisamperometricoxygensensorfrom

METTLERTOLEDO.TheInPro6000(i)seriesamperometric

O

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 sensors are intendedsolely for in-line measurement

oftheoxygenpartialpressuree.g.,oxygenmeasurement

inliquids.

Applicationexamplesare(butnotlimitedto),fermentation

in biotechnology, oxygen measurement in brewing and

chemicalapplications.

The followingsensor types arecoveredwithinthisquick

set-upguide.

InPro6800/InPro6850i/InPro6900/InPro6900i/

InPro6950/InPro6950i/easySense.

Sensorswithout’i’areanalogsensorsandwith’i’aredigital

sensorsincorporatingIntelligentSensorManagement(ISM).

EasySenseisdigitalsensorwithoutISM.ISMfunctionality

offerPlugandMeasure as well asenhanceddiagnostics

features.

2 Safety instructions

h

Notice:Beforeeverystart-up,thesensormustbechecked

for:

 –Damagetotheconnections,fastenings,etc.

 –Leakage

 –Perfectfunctioning

 –Authorization for use in conjunction with other plant

equipmentandresources.

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Notice:Themanufacturer/supplieracceptsnoresponsibility

for any damage caused by unauthorized attachments

or for the incorporation of spare parts which are not of

METTLERTOLEDOprovenance.Theriskisborneentirelyby

theoperator.

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Caution:Beforethesensorisputintooperation,the

operatormusthavealreadyclariedthatuseofthesensor

in conjunction with the other associated equipment and

resourcesisfullyauthorized.

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Caution:A defectivesensormay neitherbeinstallednor

putintooperation.Faultycontainmentorinstallationoutof

conformancewithregulationsandinstructionscanleadto

theescapeofmediumortopressuresurges(explosion),

potentiallyharmfulbothtopersonsandtotheenvironment.

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Caution: Thesensorisnotequippedwithheatprotection.

Duringsteam-sterilizationproceduresinpipes,thesurface

ofthesensorcanreachhightemperaturesandcauseburns.

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Caution: Somecomponentsinsidethesensorareenergized

withvoltages which can cause lethal shocksin case of

contact. The instrument needs to be switched to zero

potentialbeforeanyoperationonthewiringterminal.

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Warning: Beforedismantlingthesensororcommencingany

maintenanceworkonit,ensurethattheequipmentinwhich

thesensorisinstalledisinasafecondition(pressurize,

noexplosionrisk,empty,rinse,vent,etc.).

3 Product description

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Notice:Digitalsensors(ISM):Allsensorsendingwithan’i’

aredelivereddryandmustbelledwithelectrolytebefore

start-up.Electrolyte has to be ordered separately.

 Analogsensorsaredeliveredlledwithelectrolyte,however,

itisadvisedtoreplacetheelectrolytereservoirwithfresh

solution.

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Article Nr.: Electrolytes

 59907065–O

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Electrolyte25mL(InPro6050;

InPro6800;InPro6850i;easySense)

 52206107–O

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Electrolyte25mLHighSalinity

[InPro6900(i);InPro6950(i)]

 30298424–O

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electrolytepack3×25mL

(InPro6050;InPro6800;InPro6850i;

easySense)

 30298425–O

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electrolytepack–highsalinity3×25mL

[InPro6900(i);InPro6950(i)]

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Warning: The O

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electrolytehasanalkalinepHvalue.

Contactofelectrolytewithmucousmembraneoreyesis

to be avoided. Therefore protective gloves and safety

glasses have to be worn for the following dismantling

works.Ifsuchcontactoccurs,theaffectedareashouldbe

wellrinsedwithwater.Inthecaseofaccident,orshouldever

anyadversesignsappear,getimmediatemedicalattention.

4 Installation

4.1 Connection

The sensors are installed to a transmitter by using a VP

(analogsensors) or AK9 (ISMsensors) connector cable.

Cables in different lengths 2–50 m are available from

METTLERTOLEDO.

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Notice:Cableand terminal assignment can be foundin

theMETTLERTOLEDOcableand/ortransmitterinstruction

manual.

  VPconnector Slit Pin Plug VP-6cable

  K8S(ISM)    AK9(ISM)

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Transmitter VPorAK9cable

4.2 Mounting the sensor

Before mounting the sensor into a housing remove the

protectioncaponthesensor.Thesensorcanthenbemounted

intoanInFit/InTracSerieshousingfromMETTLERTOELDO.

Alternatively,the12mmsensorscan bemounteddirectly

throughasocketwithinsidethreadPg13.5andsecurely

tightenedviathePg13.5threadedsleeve.

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Notice:Forconnecting the cable tothe terminals ofthe

transmitter, please refer to the instructions given in the

METTLERTOLEDOtransmittermanual(www.mt.com/pro-

transmitters)

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5 Operation

5.1 Start-up and polarizing

Whenthesystemisoperatedforthersttimeorifthesensor

hasbeendisconnectedfromthevoltagesource(transmitter

or O

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sensormaster)forlongerthan5minutes,thesensor

hastobepolarizedpriortocalibrationbyconnectingittothe

operatingO

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transmitterortoasensormaster.After6hours,

thesensorwillbefullypolarizedandreadyforoperation.

For polarizing and storage the cleaning and conditioning

solution (order Nr. 52 200 255) is recommended. This

solutioncontainsanoxygenscavengerwhichensuresthat

theelectrolyteofthesensordoesnotcomeintocontactwith

oxygenwhennotinuse.

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Attention:TheInPro6950ishouldneverbepolarizedatair!

It is recommended to store the sensors in the according

electrolyteorcleaningandconditioningsolutionduringthe

polarizationtime.TheInPro6900iand6950iuseaspecial

electrolytewhichcontainsanoxygenscavenger.

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Warning: Setting of the polarization voltage on the

transmitter for correct measurements:

Standardapplications:–675mV.

Measurementsofcontinuouslylowestoxygenconcentrations

(<500ppb in liquids or<10,000 ppm [vol.] ingases)

andInpresenceofvolatileacidiccomponents(e.g.carbon

dioxideduringmeasurementsinbreweries):–500mV.

5.2 Calibration

WithdigitalISMsensorsallcalibrationdataarestoredinthe

sensor.Oncelledwithelectrolyteandpolarizedtheycanbe

connectedtoanISMtransmitterandimmediatelyusedfor

measurement.Analogsensorsaredeliveredwetandafter

polarizationcanbeslope1-pt,2pt-orprocesscalibrated

usingatransmitter.

With ISM sensors METTLER TOLEDO’s calibration

and maintenance software tools iSense/iSense light

are recommended for sensor checking and calibration.

(www.mt.com/iSense).

Polarizationvoltageforcalibrationpurposesarealwaysput

to–675mV.

Formeasurements incarbondioxidecontainingsolutions

the transmitter setting has to be switched to –500 mV

accordinglyafterthecalibration.

6 Maintenance

Ifthemembraneand/ortheinteriorbodyexhibitssignsof

failure(longresponsetime,increasedcurrentinanoxygen-

freemedium,mechanicaldamage,etc.)themembranebody

and/ortheinteriorbodyhastobereplaced.

The incorporated Intelligent Sensor Management (ISM)

technologymonitorsandreportstheremaininglifetimeof

theinnerbodiesastheDynamicLifetimeIndicator.

Dependingontheaggressiveness(CIP/SIP)oftheapplication

conditionsareplacementofelectrolyte,themembranebody

or the interior body is recommended. This maintenance

can be performed by using the transmitter’s calibration

menu and/or using METTLER TOLEDO’s calibration and

maintenancetooliSense(www.mt.com/iSense).

Fordetailedmaintenancedescriptionandcriteriapleaserefer

toiSenseorthemainsensormanual.

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6.1 Relling electrolyte; exchanging membrane body

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Procedure

Cleanse with demin water; turn cap sleeve twice, do not

unmountyet.Fromthebottompushthemembranebodyout

byaslightupwardspush;unscrewcompletely.Removecap

sleeveandmembranebody.Cleaninnerbody.Ifnescessary

use new membrane body and ll with fresh electrolyte

solution. Make sure no air bubbles are trapped. Replace

O-ringeachtimewhenreplacingthemembranebodyand

screwthecapsleeveoncarefully.

7 Disposal

Itistheuser’sresponsibilitytodisposeofspentspareparts

and if necessary the sensor in a professional manner.

Sensorscontainelectroniccomponentsthatrequirespecial

disposalwithoutanyhazardforhumans,andwithnoriskof

harmtotheenvironment.Pleaseobservetheapplicablelocal

ornational regulations concerning thedisposal of “waste

electricalandelectronicequipment”.

8 Warranty

Onmanufacturingdefects,12monthsafterdelivery.

9 Storage conditions

Inspect the sensor immediately after receiving for any

transportdamage.Thesensorshouldbe stored in a dry,

cleanandprotectedareauntilthetimeofinstallation.Ifthe

sensorhasbeenremovedfromthe process, it should be

thoroughlycleanedanddried.Itshouldbestoredinadry,

cleanandprotectedareauntiltimeofinstallation.

10 EC Declaration of Conformity

Thecompletedeclarationisavailableinthedeclarationof

conformitycerticate.

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6.1 Rellenado de electrolito; sustitución del cuerpo

demembrana

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6.1 Elektrolyytin täyttö; kalvon rungon vaihto

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6.1 Remplissage d’électrolyte;

remplacement ducorps à membrane

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6.1 Az elektrolit feltöltése, a membrántest cseréje

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6.1 Ricarica dell’elettrolita; sostituzione del corpo

della membrana

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60 InPro 6000 Aperometric O

2

Sensors

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6.1

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66 InPro 6000 Aperometric O

2

Sensors

30 313 395 B PrintedinSwitzerland

6.1 전해질 재충진; 멤브레인 본체 교환

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 68 InPro 6000 Aperometric O

2

Sensors

30 313 395 B PrintedinSwitzerland

1 Inleiding ........................................................................ 69

2 Veiligheidsinstructies ...................................................... 69

3 Productbeschrijving ........................................................ 69

4 Installatie ...................................................................... 70

4.1 Aansluiting .................................................................... 70

4.2 Desensormonteren ....................................................... 70

5 Bediening ..................................................................... 71

5.1 Opstartenenpolariseren ................................................. 71

5.2 Kalibratie ...................................................................... 71

6 Onderhoud .................................................................... 71

6.1 Bijvullingelektrolyt;vervangingmembraanlichaam ............ 72

7 Afvoeren ........................................................................ 73

8 Garantie ........................................................................ 73

9 Opslagomstandigheden .................................................. 73

10 EG-verklaringvanovereenstemming ................................ 73

Inhoud

InPro 6000

Amperometrische O

2

-sensoren

Beknopte handleiding

InProenISMzngedeponeerdehandelsmerken

vanMettler-ToledoGmbHinZwitserland,deVS,

deEuropeseUnieenvfanderelanden.

nl

Blage

Technischetekeningen .............................................................. 110

nl Beknoptehandleiding

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 72 InPro 6000 Aperometric O

2

Sensors

30 313 395 B PrintedinSwitzerland

6.1 Bvulling elektrolyt; vervanging membraanlichaam

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 78 InPro 6000 Aperometric O

2

Sensors

30 313 395 B PrintedinSwitzerland

6.1 Uzupełnianie elektrolitu; wymiana korpusu

membrany

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 84 InPro 6000 Aperometric O

2

Sensors

30 313 395 B PrintedinSwitzerland

6.1 Relamento de eletrólito;

troca do corpo demembrana

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Mettler Toledo InPro 6000 Amperometric O2 Sensors Operating instructions

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