Thermo Fisher Scientific Barnstead MicroPure Ultrapure Water System Operating instructions

Type
Operating instructions
Thermo Scientific
Barnstead MicroPure
Ultrapure water system
Operating Instructions
50148630 Revision B June 2016
© 2016 Thermo Fisher Scientific Inc. All rights reserved.
Thermo Fisher Scientific Inc. provides this document to its customers with a product purchase to use in the
product operation. This document is copyright protected and any reproduction of the whole or any part of this
document is strictly prohibited, except with the written authorization of Thermo Fisher Scientific Inc.
The contents of this document are subject to change without notice. All technical information in this
document is for reference purposes only. System configurations and specifications in this document supersede
all previous information received by the purchaser.
This document is not part of any sales contract between Thermo Fisher Scientific Inc. and a purchaser. This
document shall in no way govern or modify any Terms and Conditions of Sale, which Terms and Conditions of
Sale shall govern all conflicting information between the two documents.
Release history:
For Research Use Only. Not for use in diagnostic procedures.
Preface
Thermo Scientific MicroPure i
Preface
© 2016 Thermo Fisher Scientific Inc. All rights reserved.
These operating instructions are protected by copyright. Rights resulting thereof, particularly reprint,
photomechanical or digital postprocessing or reproduction, even in part, are only allowed with the
written consent of Thermo Electron LED GmbH. This regulation does not apply to reproductions for
in-plant use. The contents of this operating instructions manual may change at any time and without
any prior notice. In case of conflicting translations into foreign languages the German-language version
of these operating instructions shall be binding.
Please read through the information given in these operating instructions on installing and operating
the system before you begin installation and use of your water purification system. This is of particular
importance, as we, the manufacturer, do not assume any liability for damage due to incorrect operation
or use of the system other than the intended use.
Thermo Fisher Scientific Inc. provides this document to its customers with a product purchase to use
in the product operation. This document is copyright protected. Any reproduction of the whole or any
part of this document is strictly prohibited, except with the written authorization of Thermo Fisher
Scientific Inc. The contents of this document are subject to change without notice. All technical
information in this document is for reference purposes only. System configurations and specifications
in this document supersede all previous information received by the purchaser.
Thermo Fisher Scientific Inc. makes no representations that this document is complete, accurate or
error-free and assumes no responsibility and will not be liable for any errors, omissions, damage or loss
that might result from any use of this document, even if the information in the document is followed
properly.
This document is not part of any sales contract between Thermo Fisher Scientific Inc. and a purchaser.
This document shall in no way govern or modify any Terms and Conditions of Sale, which Terms and
Conditions of Sale shall govern all conflicting information between the two documents.
Legal Information
Warranty
Thermo Electron LED GmbH warrants the operational safety and functions of the Thermo Scientific
Barnstead Ultrapure Water Systems only under the condition that:
The system is installed and operated as per the operation manual. Do not use this product for
anything other than its intended use.
the system is not modified,
Specifications, terms and pricing are subject to change. Not all products are
available in all countries. Please consult your local sales representative for details.
Preface
ii MicroPure Thermo Scientific
only original spare parts and accessories that have been approved by Thermo Electron LED
GmbH are used (third-party spares without Thermo Electron LED GmbH approval void the
limited warranty),
inspections and maintenance are performed at the specified intervals,
an installation verification test is performed on commissioning the system for the first time and
repeated after each preventative maintenance and repair activity. The warranty is valid from the
date of delivery of the system to the customer.
The above mentioned warranty conditions are subject to the general terms and conditions of sale,
in effect at the time of purchase, which apply as well.
Preface
Thermo Scientific MicroPure iii
Explanatory notes on the operating instructions
EU Mark of Conformity
CSA - admission
Indicates a situation which, if not avoided, could result in damage to equipment
or property.
Indicates a hazardous situation which, if not avoided, could result in death or
serious injuries.
Indicates a hazardous situation which, if not avoided, will result in death or
serious injuries.
Is used for applicational hints and useful information.
Risk of electric shock. Electrical work on the system is only to be carried out by qualified personnel.
Protective conductor connection
Connect the power supply to an electrical socket with a protective connection.
Indicates a situation in which protective gloves or clothing must be worn.
Indicates a situation in which protective goggles must be worn.
Preface
iv MicroPure Thermo Scientific
This information is valid for the system that is received. For quick and correct service, please include
the following information on all inquiries and replacement parts orders which relate to your system:
the serial number (located on the back of the system on the nameplate)
•the catalog number
Standards and directives
The Therno Scientific Barnstead Ultrapure water Systems complies with the following standards and
directives:
Low Voltage Directive 2014/35/EC
EMC Directive 2014/30/EU
ASTM D1193-6
RoHs 2011/65/EU
Additionally, the ultrapure water system is in compliance with many other international standards,
regulations and directives not listed here. Should you have any questions regarding compliance with
national standards, regulations and directives applicable for your country, please contact your Thermo
Fisher Scientific sales organization.
Indicates a situation in which breathing protection must be used.
Thermo Scientific MicroPure v
C
Preface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . i
Legal Information. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ii
Warranty . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ii
Explanatory notes on the operating instructions . . . . . . . . . . . . . . . . . . . . . . . . iii
Standards and directives . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . iv
Chapter 1 Transport and packaging . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Examination on receipt . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Complaints . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Packaging for return shipment. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Chapter 2 Safety precautions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Chapter 3 Extend of delivery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
Extent of delivery MicroPure. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
Extend of delivery MicroPure with tank . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
Available MicroPure systems . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
Available MicroPure with tank systems . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
Chapter 4 Intended Use of the device. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
Intended Use. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
Unintended use . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
Chapter 5 Technical Specification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
Chapter 6 The Installation area . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
Chapter 7 Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
Connections of the MicroPure system . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
Connections of the MicroPure with tank system . . . . . . . . . . . . . . . . . . . . . . . 21
Start your MicroPure system into operation . . . . . . . . . . . . . . . . . . . . . . . . . . 22
Illustration of drain . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25
Wall Mounting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26
Mounting the power pack (voltage supply) . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
Contents
Contents
vi MicroPure Thermo Scientific
Chapter 8 Flow chart. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29
Chapter 9 How the MicroPure system functions . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31
Chapter 10 Initial start up. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
Putting system into operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34
Dispensing water from Dispensing valve . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
Venting the sterile filter . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35
Chapter 11 Operating Elements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37
Description of control display . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38
Control menu flow diagram . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39
Chapter 12 System control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41
General information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42
Operating modes. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42
Interval operating mode after switching on . . . . . . . . . . . . . . . . . . . . . . . . . . . 42
Non-stop mode . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43
Interval operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43
UV-Lamp . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44
OFF mode. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44
User menu. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45
Feedwater limiting value . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45
Ultrapure water limiting value. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46
UV-Lamp operating time . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
Ultrapure cartridge operating hours counter . . . . . . . . . . . . . . . . . . . . . . . . . . 47
Rinsing Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47
Disinfection Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49
Error history . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50
Print out of Data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50
Entering a code number . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51
Code lock . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51
OEM Menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52
Set the limiting value for temperature . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52
Set the rinsing time . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53
Change the disinfection time. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53
Set the interval pump time . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53
Set the interval rinse time . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54
Set the real-time clock . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54
Set the sending interval . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54
Language selection. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55
Switch units, conductivity/resistance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55
Switch temperature compensation on/off . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55
Printer output . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55
Contents
Thermo Scientific MicroPure vii
Chapter 13 Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 57
Maintenance intervals . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58
Replacing the ultrapure cartridge. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59
Disinfection of MicroPure system . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61
Disinfection of MicroPure with tank system . . . . . . . . . . . . . . . . . . . . . . . . . . 64
Replacing the ultrafilter . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65
UV-reactor assembly . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68
Replacing the UV-lamp. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69
Replacing the final end filter (0.2μm) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72
Autoclaving the final end filter . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72
Chapter 14 Waste disposal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 73
Chapter 15 Trouble shooting. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 75
Chapter 16 Replacement parts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 79
Replacement parts MicroPure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 80
Replacement parts MicroPure with tank . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 82
Chapter 17 Consumables. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 85
Accessories. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 85
Chapter 18 Terminal assignment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 87
Chapter 19 Maintenance record. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 89
Chapter 20 Contact information Thermo Fisher Scientific . . . . . . . . . . . . . . . . . . . . . 91
Contents
viii MicroPure Thermo Scientific
1 Transport and packaging
Thermo Scientific MicroPure 1
Transport and packaging
Content
“Examination on receipton page 2
“Complaintson page 2
“Packaging for return shipment” on page 2
Do not pull the plastic foil over your head. Risk of suffocation.
Use the plastic foil only for packaging.
1 Transport and packaging
2MicroPure Thermo Scientific
Ultrapure water systems are carefully inspected and packed prior to shipping, but damage
could still possibly occur during transport. Lifting and carrying the Thermo Scientific
Barnstead Ultrapure Water System, e.g. to the installation location, should be carried out by
two people.
Examination on receipt
Check the completeness of the goods received against the packing list.
Complaints
Should damage have occurred to the goods during transport:
Immediately contact your delivery transport agency.
Save the complete packaging, including the cardboard box, for a possible inspection of
them and/or return shipment of the system.
Packaging for return shipment
If possible, use the original box and packaging material.
When these are no longer available, then:
Protect the system from shock by packing it in bubble wrap and/or packaging foam and a
strong cardboard box.
Does the packaging show signs of damage? Inspect the system for damage.
Packaging
System
The time limit for claims is 6 days from the time of receipt of the goods. The right
to claim for damages ceases when this time has elapsed.
Only a trained person should take the system out of operation.
Prior to send back a operated device, empty the water and dry the system and
take out the cartridges.
pack the ultrapure cartridges into a bubble wrap and/or packaging foam and
take it with in into the package of the ultrapure water system.
2 Safety precautions
Thermo Scientific MicroPure 3
Safety precautions
Do not install or operate the system until you have carefully read through these operating
instructions and the notes and notices contained therein.
Lifting and carrying the ultrapure water system, e.g. to the installation location, should be
carried out by two people. To do this, lift the system in tandem at the two corner points
beneath the bottom plate.
The CE mark is nullified if you make any structural changes to the system or install
products from other manufacturers in/on the system.
Protect the system from frost. The temperature at the installation area must be between
+2 °C and +40 °C.
Always observe the applicable, pertinent codes and regulations valid at the installation
location of the system and follow all applicable accident prevention regulations.
The feedwater pressure must be at least 0.1 bar and at max. 6 bar or 1.45 to 87 PSI.
When the feedwater pressure is higher, install an external pressure reducer.
A low pressure check valve is recommended to prevent back flow of feedwater from water
system.
A grounded 100-240V, 50/60Hz electrical outlet must be available (see “Electrical
connectionson page 15).
Access to the power supply cord and plug may never be restricted or obstructed.
Unplug the system from the power outlet for all maintenance work on the system.
Observe these safety precautions for your own safety!
The Thermo Scientific Barnstead Ultrapure Water Systems are modern water
purification system intended solely for the treatment of potable water. The water it
produces is not fit for drinking.
Work may only be performed on the system electronics when the system has been
switched off and when ESD protection is in place. Only specially trained personnel
may work on the system‘s electronics.
2 Safety precautions
4MicroPure Thermo Scientific
An atmospherically vented floor drain with a nominal outer diameter of at least 63 mm
(2.48 inch) (DN50 tube) must be present at the installation location. If no drain is
provided it is recommended to install for safety reasons a water watcher (for European
specifications only). Failure to provide this will release the manufacturer from liability for
any water-induced damage that may result.
Proceed as follows if the system is not to be operated for an extended period, e.g., over
extended weekend, or during a vacation period:
Switch the system off (unplug the mains plug).
Close the feedwater inlet (close the feedwater tap).
The pump would be damaged if the system were to run without any supply of feedwater.
The manufacturer will not accept any liability should this occur.
The system must be disinfected or rinsed after an extended down time. The disinfection
procedure is described under “Disinfection of MicroPure systemon page 61.
The surface or wall on which the system is to be installed or mounted must have an
adequate load-carrying capacity (check the capacity and stability of the wall). The dry
weight of the system is given under “Dimensions and weight of MicroPureon page 15
and “Dimensions and weight MicroPure with tankon page 13. When the internal tank
is filled, the system has a weight during operation of approx. 32 kg / 70.55 lbs.
The surface on which the system is installed must be level and stable-not to exceed a
maximum of 2% deviation from evenness is recommended.
When installing the water purification system, always ensure that there is adequate space
all around the system (see Accessibility to MicroPure systemon page 16) to ensure that
ease of use or easy replacement of materials (e.g., filter change, connection) is possible at
all times.
Visually inspect the system at regular intervals. Clean up any water or spills found around the
system immediately.
Never look directly into a switched-on UV-lamp, as UV-light endangers eyesight!
To avoid the risk of pinching, crushing, cutting or electrical shock, never perform
maintenance on the system without its protective housing, or while it is in operation.
Maintenance work on the system may only be performed by trained, authorized
specialists.
2 Safety precautions
Thermo Scientific MicroPure 5
.
To avoid tripping, ensure that the tubings do not lay over the floor.
Apply the general rules of hygiene for laboratories when working with the system.
Do not use any oxidative cleaning agents for cleaning the system. These can damage the
system.
Proceed as follows when the system has a defect:
Switch the system off and unplug the system from power outlet.
Shut off the feedwater supply.
Contact your local service organization.
Wear safety gloves when working with disinfectant solutions.
If your skin should come into contact with a chlorine product, rinse it immediately with ample,
fresh water.
The system, or system components, may heat up as a result of a defect. It is recommended to
always wear appropriate safety gloves to prevent skin damage or burns.
Wear safety gloves when changing the UV-lamp, in order to prevent that your skin comes in
contact with the UV-lamp glass.
Wear safety glasses when working with disinfectant solutions.
If your eyes come into contact with a chlorine product, rinse them immediately with ample,
fresh water and immediately contact a physician.
Check the UV-lamp before initial start.
•If the UV-lamp is broken
wear a breathing protector, filter category FFP3 and replace the UV-lamp. For disposal the
UV-lamp refer to “Waste disposal” on page 73.
ventilate the room well.
The Hg content in the UV-lamp is so low so that no damage to the
environment can arise.
2 Safety precautions
6MicroPure Thermo Scientific
3 Extend of delivery
Thermo Scientific MicroPure 7
Extend of delivery
Contents
“Extent of delivery MicroPure” on page 8
“Extend of delivery MicroPure with tankon page 8
Available MicroPure systemson page 9
Available MicroPure with tank systemson page 9
3 Extend of delivery
8MicroPure Thermo Scientific
Extent of delivery MicroPure
The following items are included with the MicroPure ultrapure water system.
1x MicroPure ultrapure water system Item No.: 5013xxxx
1x Ultrapure cartridge Item No.: 09.1006
including 1 x assembly kit
consisting of:
1x Final end filter (sterile filter 0.2μm) Item No.: 09.1003
1x Feedwater connecting kit Item No.: 25.0075
1x Rinse water tube, o.d 8 mm/0.31inch, 3m Item No.: 18.0036
1x Table top power pack Item No.: 50149597
1x Universal holder Item No.: 21.1007
1x Universal adapter Item No.: 21.1006
1x Rubber connector to nema plug connector Item No.: 50132200
1x Rubber connector to british ST plug connector Item No.: 50132203
1x Rubber connector to euro plug connector Item No.: 50132215
Extend of delivery MicroPure with tank
The following items are included with the MicroPure ultrapure water system.
1x MicroPure with tank Item No.:5013xxxx
1x Ultrapure cartridge Item No.: 09.1006
including 1x assembly kit
consisting of:
1x Final end filter (sterile filter 0.2μm) Item No.: 09.1003
1x Rinse water tube, o.d 8 mm/0.31inch, 3m Item No.: 18.0036
1x Table top power pack Item No.: 50149597
1x Universal holder Item No.: 21.1007
1x Universal adapter Item No.: 21.1006
1x Rubber connector to nema plug connector Item No.: 50132200
1x Rubber connector to british ST plug connector Item No.: 50132203
1x Rubber connector to euro plug connector Item No.: 50132215
3 Extend of delivery
Thermo Scientific MicroPure 9
Available MicroPure systems
Available MicroPure with tank systems
Item No.: System Equipment
50132366 MicroPure standard
50132368 MicroPure UF
50132370 MicroPure UV/UF
50132373 MicroPure UV
Item No.: System Equipment
50132367 MicroPure with tank standard
50132369 MicroPure with tank UF
50132372 MicroPure with tank UV/UF
50132374 MicroPure with tank UV
3 Extend of delivery
10 MicroPure Thermo Scientific
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Thermo Fisher Scientific Barnstead MicroPure Ultrapure Water System Operating instructions

Type
Operating instructions

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