Thermo Fisher Scientific Barnstead MicroPure Ultrapure Water System Operating instructions

Thermo Scientific

Barnstead MicroPure

Ultrapure water system

Operating Instructions

50148630 Revision B June 2016

Thermo Fisher Scientific Inc. provides this document to its customers with a product purchase to use in the

product operation. This document is copyright protected and any reproduction of the whole or any part of this

document is strictly prohibited, except with the written authorization of Thermo Fisher Scientific Inc.

The contents of this document are subject to change without notice. All technical information in this

document is for reference purposes only. System configurations and specifications in this document supersede

all previous information received by the purchaser.

This document is not part of any sales contract between Thermo Fisher Scientific Inc. and a purchaser. This

document shall in no way govern or modify any Terms and Conditions of Sale, which Terms and Conditions of

Sale shall govern all conflicting information between the two documents.

Release history:

For Research Use Only. Not for use in diagnostic procedures.

Preface

Thermo Scientific MicroPure i

Preface

These operating instructions are protected by copyright. Rights resulting thereof, particularly reprint,

photomechanical or digital postprocessing or reproduction, even in part, are only allowed with the

written consent of Thermo Electron LED GmbH. This regulation does not apply to reproductions for

in-plant use. The contents of this operating instructions manual may change at any time and without

any prior notice. In case of conflicting translations into foreign languages the German-language version

of these operating instructions shall be binding.

Please read through the information given in these operating instructions on installing and operating

the system before you begin installation and use of your water purification system. This is of particular

importance, as we, the manufacturer, do not assume any liability for damage due to incorrect operation

or use of the system other than the intended use.

Thermo Fisher Scientific Inc. provides this document to its customers with a product purchase to use

in the product operation. This document is copyright protected. Any reproduction of the whole or any

part of this document is strictly prohibited, except with the written authorization of Thermo Fisher

Scientific Inc. The contents of this document are subject to change without notice. All technical

information in this document is for reference purposes only. System configurations and specifications

in this document supersede all previous information received by the purchaser.

Thermo Fisher Scientific Inc. makes no representations that this document is complete, accurate or

error-free and assumes no responsibility and will not be liable for any errors, omissions, damage or loss

that might result from any use of this document, even if the information in the document is followed

properly.

This document is not part of any sales contract between Thermo Fisher Scientific Inc. and a purchaser.

This document shall in no way govern or modify any Terms and Conditions of Sale, which Terms and

Conditions of Sale shall govern all conflicting information between the two documents.

Legal Information

Warranty

Thermo Electron LED GmbH warrants the operational safety and functions of the Thermo Scientific

Barnstead Ultrapure Water Systems only under the condition that:

• The system is installed and operated as per the operation manual. Do not use this product for

anything other than its intended use.

• the system is not modified,



Specifications, terms and pricing are subject to change. Not all products are

available in all countries. Please consult your local sales representative for details.

Preface

ii MicroPure Thermo Scientific

• only original spare parts and accessories that have been approved by Thermo Electron LED

GmbH are used (third-party spares without Thermo Electron LED GmbH approval void the

limited warranty),

• inspections and maintenance are performed at the specified intervals,

• an installation verification test is performed on commissioning the system for the first time and

repeated after each preventative maintenance and repair activity. The warranty is valid from the

date of delivery of the system to the customer.

• The above mentioned warranty conditions are subject to the general terms and conditions of sale,

in effect at the time of purchase, which apply as well.

Preface

Thermo Scientific MicroPure iii

Explanatory notes on the operating instructions

EU Mark of Conformity

CSA - admission



Indicates a situation which, if not avoided, could result in damage to equipment

or property.



Indicates a hazardous situation which, if not avoided, could result in death or

serious injuries.



Indicates a hazardous situation which, if not avoided, will result in death or

serious injuries.



Is used for applicational hints and useful information.



Risk of electric shock. Electrical work on the system is only to be carried out by qualified personnel.

Protective conductor connection

Connect the power supply to an electrical socket with a protective connection.



Indicates a situation in which protective gloves or clothing must be worn.



Indicates a situation in which protective goggles must be worn.

Preface

iv MicroPure Thermo Scientific

This information is valid for the system that is received. For quick and correct service, please include

the following information on all inquiries and replacement parts orders which relate to your system:

• the serial number (located on the back of the system on the nameplate)

•the catalog number

Standards and directives

The Therno Scientific Barnstead Ultrapure water Systems complies with the following standards and

directives:

• Low Voltage Directive 2014/35/EC

• EMC Directive 2014/30/EU

• ASTM D1193-6

• RoHs 2011/65/EU

Additionally, the ultrapure water system is in compliance with many other international standards,

regulations and directives not listed here. Should you have any questions regarding compliance with

national standards, regulations and directives applicable for your country, please contact your Thermo

Fisher Scientific sales organization.



Indicates a situation in which breathing protection must be used.

Thermo Scientific MicroPure v

C

Preface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . i

Legal Information. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ii

Warranty . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ii

Explanatory notes on the operating instructions . . . . . . . . . . . . . . . . . . . . . . . . iii

Standards and directives . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . iv

Chapter 1 Transport and packaging . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Examination on receipt . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Complaints . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Packaging for return shipment. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Chapter 2 Safety precautions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Chapter 3 Extend of delivery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

Extent of delivery MicroPure. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Extend of delivery MicroPure with tank . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Available MicroPure systems . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Available MicroPure with tank systems . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Chapter 4 Intended Use of the device. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

Intended Use. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

Unintended use . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

Chapter 5 Technical Specification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

Chapter 6 The Installation area . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

Chapter 7 Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19

Connections of the MicroPure system . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20

Connections of the MicroPure with tank system . . . . . . . . . . . . . . . . . . . . . . . 21

Start your MicroPure system into operation . . . . . . . . . . . . . . . . . . . . . . . . . . 22

Illustration of drain . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25

Wall Mounting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26

Mounting the power pack (voltage supply) . . . . . . . . . . . . . . . . . . . . . . . . . . . 27

Contents

vi MicroPure Thermo Scientific

Chapter 8 Flow chart. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29

Chapter 9 How the MicroPure system functions . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31

Chapter 10 Initial start up. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33

Putting system into operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34

Dispensing water from Dispensing valve . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35

Venting the sterile filter . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35

Chapter 11 Operating Elements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37

Description of control display . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38

Control menu flow diagram . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39

Chapter 12 System control . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41

General information . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42

Operating modes. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42

Interval operating mode after switching on . . . . . . . . . . . . . . . . . . . . . . . . . . . 42

Non-stop mode . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43

Interval operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43

UV-Lamp . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44

OFF mode. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44

User menu. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45

Feedwater limiting value . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45

Ultrapure water limiting value. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46

UV-Lamp operating time . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47

Ultrapure cartridge operating hours counter . . . . . . . . . . . . . . . . . . . . . . . . . . 47

Rinsing Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47

Disinfection Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49

Error history . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50

Print out of Data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50

Entering a code number . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51

Code lock . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51

OEM Menu . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52

Set the limiting value for temperature . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52

Set the rinsing time . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53

Change the disinfection time. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53

Set the interval pump time . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53

Set the interval rinse time . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54

Set the real-time clock . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54

Set the sending interval . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54

Language selection. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55

Switch units, conductivity/resistance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55

Switch temperature compensation on/off . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55

Printer output . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55

Contents

Thermo Scientific MicroPure vii

Chapter 13 Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 57

Maintenance intervals . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58

Replacing the ultrapure cartridge. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59

Disinfection of MicroPure system . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61

Disinfection of MicroPure with tank system . . . . . . . . . . . . . . . . . . . . . . . . . . 64

Replacing the ultrafilter . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65

UV-reactor assembly . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68

Replacing the UV-lamp. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69

Replacing the final end filter (0.2μm) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72

Autoclaving the final end filter . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72

Chapter 14 Waste disposal . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 73

Chapter 15 Trouble shooting. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 75

Chapter 16 Replacement parts . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 79

Replacement parts MicroPure . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 80

Replacement parts MicroPure with tank . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 82

Chapter 17 Consumables. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 85

Accessories. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 85

Chapter 18 Terminal assignment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 87

Chapter 19 Maintenance record. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 89

Chapter 20 Contact information Thermo Fisher Scientific . . . . . . . . . . . . . . . . . . . . . 91

Contents

viii MicroPure Thermo Scientific

1 Transport and packaging

Thermo Scientific MicroPure 1

Transport and packaging

Content

•“Examination on receipt” on page 2

•“Complaints” on page 2

•“Packaging for return shipment” on page 2

Do not pull the plastic foil over your head. Risk of suffocation.

Use the plastic foil only for packaging.

1 Transport and packaging

2MicroPure Thermo Scientific

Ultrapure water systems are carefully inspected and packed prior to shipping, but damage

could still possibly occur during transport. Lifting and carrying the Thermo Scientific

Barnstead Ultrapure Water System, e.g. to the installation location, should be carried out by

two people.

Examination on receipt

Check the completeness of the goods received against the packing list.

Complaints

Should damage have occurred to the goods during transport:

• Immediately contact your delivery transport agency.

• Save the complete packaging, including the cardboard box, for a possible inspection of

them and/or return shipment of the system.

Packaging for return shipment

If possible, use the original box and packaging material.

When these are no longer available, then:

Protect the system from shock by packing it in bubble wrap and/or packaging foam and a

strong cardboard box.

Does the packaging show signs of damage? Inspect the system for damage.

Packaging

System

The time limit for claims is 6 days from the time of receipt of the goods. The right

to claim for damages ceases when this time has elapsed.

• Only a trained person should take the system out of operation.

• Prior to send back a operated device, empty the water and dry the system and

take out the cartridges.

• pack the ultrapure cartridges into a bubble wrap and/or packaging foam and

take it with in into the package of the ultrapure water system.

2 Safety precautions

Thermo Scientific MicroPure 3

Safety precautions

• Do not install or operate the system until you have carefully read through these operating

instructions and the notes and notices contained therein.

• Lifting and carrying the ultrapure water system, e.g. to the installation location, should be

carried out by two people. To do this, lift the system in tandem at the two corner points

beneath the bottom plate.

• The CE mark is nullified if you make any structural changes to the system or install

products from other manufacturers in/on the system.

• Protect the system from frost. The temperature at the installation area must be between

+2 °C and +40 °C.

• Always observe the applicable, pertinent codes and regulations valid at the installation

location of the system and follow all applicable accident prevention regulations.

• The feedwater pressure must be at least 0.1 bar and at max. 6 bar or 1.45 to 87 PSI.

When the feedwater pressure is higher, install an external pressure reducer.

• A low pressure check valve is recommended to prevent back flow of feedwater from water

system.

• A grounded 100-240V, 50/60Hz electrical outlet must be available (see “Electrical

connections” on page 15).

• Access to the power supply cord and plug may never be restricted or obstructed.

• Unplug the system from the power outlet for all maintenance work on the system.

Observe these safety precautions for your own safety!

The Thermo Scientific Barnstead Ultrapure Water Systems are modern water

purification system intended solely for the treatment of potable water. The water it

produces is not fit for drinking.

Work may only be performed on the system electronics when the system has been

switched off and when ESD protection is in place. Only specially trained personnel

may work on the system‘s electronics.

2 Safety precautions

4MicroPure Thermo Scientific

• An atmospherically vented floor drain with a nominal outer diameter of at least 63 mm

(2.48 inch) (DN50 tube) must be present at the installation location. If no drain is

provided it is recommended to install for safety reasons a water watcher (for European

specifications only). Failure to provide this will release the manufacturer from liability for

any water-induced damage that may result.

• Proceed as follows if the system is not to be operated for an extended period, e.g., over

extended weekend, or during a vacation period:

• Switch the system off (unplug the mains plug).

• Close the feedwater inlet (close the feedwater tap).

The pump would be damaged if the system were to run without any supply of feedwater.

The manufacturer will not accept any liability should this occur.

• The system must be disinfected or rinsed after an extended down time. The disinfection

procedure is described under “Disinfection of MicroPure system” on page 61.

• The surface or wall on which the system is to be installed or mounted must have an

adequate load-carrying capacity (check the capacity and stability of the wall). The dry

weight of the system is given under “Dimensions and weight of MicroPure” on page 15

and “Dimensions and weight MicroPure with tank” on page 13. When the internal tank

is filled, the system has a weight during operation of approx. 32 kg / 70.55 lbs.

• The surface on which the system is installed must be level and stable-not to exceed a

maximum of 2% deviation from evenness is recommended.

• When installing the water purification system, always ensure that there is adequate space

all around the system (see “Accessibility to MicroPure system” on page 16) to ensure that

ease of use or easy replacement of materials (e.g., filter change, connection) is possible at

all times.

Visually inspect the system at regular intervals. Clean up any water or spills found around the

system immediately.

Never look directly into a switched-on UV-lamp, as UV-light endangers eyesight!

To avoid the risk of pinching, crushing, cutting or electrical shock, never perform

maintenance on the system without its protective housing, or while it is in operation.

Maintenance work on the system may only be performed by trained, authorized

specialists.

2 Safety precautions

Thermo Scientific MicroPure 5

.

• To avoid tripping, ensure that the tubings do not lay over the floor.

• Apply the general rules of hygiene for laboratories when working with the system.

• Do not use any oxidative cleaning agents for cleaning the system. These can damage the

system.

• Proceed as follows when the system has a defect:

• Switch the system off and unplug the system from power outlet.

• Shut off the feedwater supply.

• Contact your local service organization.

• Wear safety gloves when working with disinfectant solutions.

• If your skin should come into contact with a chlorine product, rinse it immediately with ample,

fresh water.

• The system, or system components, may heat up as a result of a defect. It is recommended to

always wear appropriate safety gloves to prevent skin damage or burns.

• Wear safety gloves when changing the UV-lamp, in order to prevent that your skin comes in

contact with the UV-lamp glass.

• Wear safety glasses when working with disinfectant solutions.

• If your eyes come into contact with a chlorine product, rinse them immediately with ample,

fresh water and immediately contact a physician.

• Check the UV-lamp before initial start.

•If the UV-lamp is broken

wear a breathing protector, filter category FFP3 and replace the UV-lamp. For disposal the

UV-lamp refer to “Waste disposal” on page 73.

ventilate the room well.

The Hg content in the UV-lamp is so low so that no damage to the

environment can arise.

2 Safety precautions

6MicroPure Thermo Scientific

3 Extend of delivery

Thermo Scientific MicroPure 7

Extend of delivery

Contents

•“Extent of delivery MicroPure” on page 8

•“Extend of delivery MicroPure with tank” on page 8

•“Available MicroPure systems” on page 9

•“Available MicroPure with tank systems” on page 9

3 Extend of delivery

8MicroPure Thermo Scientific

Extent of delivery MicroPure

The following items are included with the MicroPure ultrapure water system.

1x MicroPure ultrapure water system Item No.: 5013xxxx

1x Ultrapure cartridge Item No.: 09.1006

including 1 x assembly kit

consisting of:

1x Final end filter (sterile filter 0.2μm) Item No.: 09.1003

1x Feedwater connecting kit Item No.: 25.0075

1x Rinse water tube, o.d 8 mm/0.31inch, 3m Item No.: 18.0036

1x Table top power pack Item No.: 50149597

1x Universal holder Item No.: 21.1007

1x Universal adapter Item No.: 21.1006

1x Rubber connector to nema plug connector Item No.: 50132200

1x Rubber connector to british ST plug connector Item No.: 50132203

1x Rubber connector to euro plug connector Item No.: 50132215

Extend of delivery MicroPure with tank

The following items are included with the MicroPure ultrapure water system.

1x MicroPure with tank Item No.:5013xxxx

1x Ultrapure cartridge Item No.: 09.1006

including 1x assembly kit

consisting of:

1x Final end filter (sterile filter 0.2μm) Item No.: 09.1003

1x Rinse water tube, o.d 8 mm/0.31inch, 3m Item No.: 18.0036

1x Table top power pack Item No.: 50149597

1x Universal holder Item No.: 21.1007

1x Universal adapter Item No.: 21.1006

1x Rubber connector to nema plug connector Item No.: 50132200

1x Rubber connector to british ST plug connector Item No.: 50132203

1x Rubber connector to euro plug connector Item No.: 50132215

3 Extend of delivery

Thermo Scientific MicroPure 9

Available MicroPure systems

Available MicroPure with tank systems

Item No.: System Equipment

50132366 MicroPure standard

50132368 MicroPure UF

50132370 MicroPure UV/UF

50132373 MicroPure UV

Item No.: System Equipment

50132367 MicroPure with tank standard

50132369 MicroPure with tank UF

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3 Extend of delivery

10 MicroPure Thermo Scientific

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