Thermo Fisher Scientific TriPlus Automatic Sampling System Operating instructions

Type
Operating instructions
Thermo Scientific
TriPlus
Automatic Sampling System
Operating Manual
PN 317 094 41, Revision May 2010
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Triplus Automatic Sampling System Operating Manual
Edition May 2010
Part Number 317 094 41 
© 2007-2010 Thermo Fisher Scientific Inc. All rights reserved.
Printed in ITALY.
Published by Thermo Fisher Scientific S.p.A, Technical Documentation, Strada Rivoltana 20090 Rodano (Milan) - Italy
Tel: 02 95059 373 Fax: 02 95059276
Printing History: First edition, released July 2004
Second edition, released July 2004
Third edition, released November 2004
Fourth edition, released March 2005
Fifth edition, released September 2005
Sixth edition, released December 2005
Seventh edition, released June 2006
Eighth edition, released January 2007
Ninth edition, released May 2007
Tenth edition, released December 2007
Eleventh edition, released April 2008
Twelfth edition, released July 2008
Thirteenth edition, released April 2009
Fourteenth edition, released September 2009
Fifteenth edition, released May 2010
Disclaimer
Technical Information contained in this publication is for reference purposes only and is subject to change without notice. Every effort has
been made to supply complete and accurate information; however, Thermo Fisher Scientific assumes no responsibility and will not be liable
for any errors, omissions, damage, or loss that might result from any use of this manual or the information contained therein (even if this
information is properly followed and problems still arise).
This publication is not part of the Agreement of Sale between Thermo Fisher Scientific and the purchaser of a Thermo Fisher Scientific
system. In the event of any conflict between the provisions of this document and those contained in Thermo Fisher Scientific’s Terms and
Conditions, the provisions of the Terms and Conditions shall govern.
Reference to System Configurations and Specifications supercede all previous information and are subject to change without notice.
Trademarks
TRACEâ„¢ GC Ultra, FOCUSâ„¢ GC and TriPlusâ„¢ are trademarks of Thermo Fisher Scientific Inc, and its subsidiaries. Other product names
or marks may be registered names or trademarks of other companies.
Read the manual before operating with the instrument.
Operating Manual 3
Declaration
Manufacturer: Thermo Fisher Scientific
Thermo Fisher Scientific is the manufacturer of the instrument described in this
manual and, as such, is responsible for the instrument safety, reliability and
performance only if:
• installation
• re-calibration
• changes and repairs
have been carried out by authorized personnel and if:
• the local installation complies with local law regulations
•the instrument is used according to the instructions provided and if its
operation is only entrusted to qualified trained personnel
Thermo Fisher Scientific is not liable for any damages derived from the
non-compliance with the aforementioned recommendations.
4Operating Manual
Operating Manual 5
Contents
About This Manual................................................................................................................................21
Overview..................................................................................................................................21
Conventions Used in This Manual...........................................................................................22
Instrument Markings and Symbols ..........................................................................................25
Chapter 1
Introduction........................................................................................................................................ 27
Classification of the Instrument...............................................................................................28
Environmental Conditions.............................................................................28
Safety Information ...................................................................................................................28
Crossrails Locking Screws.............................................................................29
The TriPlus Sampler ................................................................................................................30
Sampling Unit.............................................................................................................30
Sampler Support ............................................................................................30
Crossrails (X and Y axes)..............................................................................30
Turret..............................................................................................................31
Injection Assembly (Z axis)...........................................................................31
Components ................................................................................................................31
Washing Station .............................................................................................31
Fast Washing Station......................................................................................31
Tray Holder....................................................................................................32
Sample Tray...................................................................................................32
Second Sample Tray......................................................................................32
Incubation Oven (Agitator)............................................................................33
Fiber Conditioning Station.............................................................................33
Bar Code Reader............................................................................................33
Fan Station.....................................................................................................33
Power Module.............................................................................................................33
User Interface..............................................................................................................34
On-Column Injector Actuator.....................................................................................34
References...................................................................................................................34
Sampler Configuration.............................................................................................................35
TriPlus AS for Liquids................................................................................................35
TriPlus HS for Head Space.........................................................................................37
TriPlus SPME for Solid Phase Micro Extraction........................................................38
Technical Specifications ..........................................................................................................39
6Operating Manual
Contents
Chapter 2
System Description............................................................................................................................41
Crossrails ................................................................................................................................. 42
Crossrail X.................................................................................................................. 43
Crossrail Y.................................................................................................................. 43
Rear of the Sampling Unit.......................................................................................................4
4
Turret ....................................................................................................................................... 46
Injection Assembly (Z axis) ....................................................................................... 47
Injection Device....................................................................................................................... 49
Injection Device for TriPlus AS................................................................................. 49
Sliding Plate................................................................................................... 49
Syringe Holders............................................................................................. 50
Syringe........................................................................................................... 50
Syringe Volume Selector............................................................................... 51
Retractile Mechanism and Touch Sensor...................................................... 51
Injection Device for TriPlus HS................................................................................. 53
Sliding Plate................................................................................................... 53
Heated Syringe Holder.................................................................................. 53
Vial Capture Device...................................................................................... 54
Syringe........................................................................................................... 55
Syringe Volume Selector............................................................................... 55
Injection Device for TriPlus SPME............................................................................ 56
Sliding Plate................................................................................................... 56
Syringe Holder............................................................................................... 57
Vial Capture Device...................................................................................... 58
Supelco Fiber Holder..................................................................................... 59
Washing Station....................................................................................................................... 60
Fast Washing Station............................................................................................................... 63
Tray Holders and Sample Trays.............................................................................................. 64
Standard Tray Holder ................................................................................................. 64
Sample Trays for Standard Tray Holder ....................................................... 65
Thermostatted Tray Holder ........................................................................................ 70
Sample Trays for Thermostatted Tray Holder............................................... 71
Vials............................................................................................................................ 75
Well Plates.................................................................................................................. 75
Incubation Oven (Agitator)......................................................................................................7
6
MHE Device............................................................................................................... 77
Sliding Cover Replacement........................................................................... 77
Contents
Operating Manual 7
Pressure Regulator ......................................................................................................79
Bar Code Reader......................................................................................................................80
Fan Station ...............................................................................................................................83
Fiber Conditioning Station.......................................................................................................84
Status LED...............................................................................................................................86
Infrared Transceiver.................................................................................................................87
Power Module..........................................................................................................................88
Front Panel.....................................................................................................88
Rear Panel......................................................................................................88
Electrical Specifications.................................................................................90
Voltage Selector.............................................................................................90
Changing Voltage Configuration...................................................................90
On-Column Injector Actuator..................................................................................................92
Chapter 3
Installation on Thermo GCs.............................................................................................................. 95
Preliminary Information...........................................................................................................97
Who Performs the Installation ....................................................................................97
Space Requirements....................................................................................................97
Electrical Requirements..............................................................................................97
How to Lift and Carry the Crossrails X and Y ...........................................................98
Sampler Supports........................................................................................................98
Material Required for the Installation.........................................................................98
Installation References................................................................................................98
Installation of the Sampler on the GC......................................................................................99
Supports Installation on the GC................................................................................100
Sampler and Sampler Components Installation........................................................121
Syringe Holder Installation.......................................................................................136
Pneumatic Connections..........................................................................................................142
Electrical Connections ...........................................................................................................144
Power Module...........................................................................................................144
Cables Connection ....................................................................................................144
Instrument Start-up.................................................................................................................148
Sampler Alignments...............................................................................................................149
Chapter 4
Installation on Third-Party GCs........................................................................................................ 151
Preliminary Information.........................................................................................................153
8Operating Manual
Contents
Who Performs the Installation.................................................................................. 153
Space Requirements ................................................................................................. 153
Electrical Requirements............................................................................................ 153
How to Lift and Carry the Crossrails X and Y......................................................... 154
Sampler Supports...................................................................................................... 154
Material Required for the Installation ...................................................................... 154
Installation References ............................................................................................. 154
Installation of the Sampler on the GC................................................................................... 155
Supports Installation on the Agilent 5890 GC.......................................................... 156
Supports Installation on the Agilent 6850 GC.......................................................... 163
Supports Installation on the Agilent 6890 GC.......................................................... 171
Sampler and Sampler Components Installation........................................................ 179
Syringe Holder Installation....................................................................................... 194
Pneumatic Connections ......................................................................................................... 200
Electrical Connections........................................................................................................... 202
Power Module........................................................................................................... 202
Cables Connection.................................................................................................... 202
Instrument Start-up................................................................................................................ 206
Sampler Alignments ..............................................................................................................2
07
Chapter 5
TriPlus Control from the PC ..............................................................................................................209
Introduction............................................................................................................................ 210
Stand-alone Software Initial Page ......................................................................................... 211
File Menu.................................................................................................................. 211
Commands Menu...................................................................................................... 212
Start batch of samples.................................................................................. 212
Stop batch of samples.................................................................................. 213
Multiple batches .......................................................................................... 213
Start syringe solvent wash........................................................................... 214
Direct command Menu............................................................................................. 215
Help Menu................................................................................................................ 216
About........................................................................................................... 216
Related Topics.......................................................................................................... 216
Configuration Page................................................................................................................ 217
Mode......................................................................................................................... 217
Instrument Main .......................................................................................... 217
Instrument Virtual (Secondary)................................................................... 218
Contents
Operating Manual 9
Working mode .............................................................................................218
Disable hand-held control............................................................................218
Port............................................................................................................................218
RS232...........................................................................................................218
COM Port.....................................................................................................219
Ethernet........................................................................................................219
IP Address....................................................................................................219
Advanced Button .........................................................................................219
Sequence Error Handling..........................................................................................219
Error Mode...................................................................................................219
Handshake Boxes......................................................................................................220
Enable input.................................................................................................220
Inject out ......................................................................................................220
Anticipated synch before incub. End...........................................................220
Rapid Mode..................................................................................................220
Buttons......................................................................................................................220
Get................................................................................................................220
Ok.................................................................................................................221
Cancel ..........................................................................................................221
Sampler Set-up Page..............................................................................................................222
Window Grid.............................................................................................................222
ID .................................................................................................................222
Component name.........................................................................................222
In use............................................................................................................222
Help..............................................................................................................223
Buttons......................................................................................................................223
Add component............................................................................................223
Delete component ........................................................................................223
Set component..............................................................................................223
Close ............................................................................................................223
Fiber Zero Adjustment..............................................................................................224
Start adjustment procedure ..........................................................................224
Set Fiber Exposure.......................................................................................225
Exit...............................................................................................................225
X-Axis Driver ...........................................................................................................226
Home Position..............................................................................................226
Rapid Mode Advanced Parameters..............................................................227
Related Topics...........................................................................................................228
10 Operating Manual
Contents
Component Information Page................................................................................................ 229
Component Position ................................................................................................. 229
Other information..................................................................................................... 229
Parameter Setting Group Box................................................................................... 229
Check Box of the selected component ........................................................ 229
Z height tolerance (mm).............................................................................. 230
Goto Commands....................................................................................................... 230
When Washing Station is selected .............................................................. 230
When Tray holder is selected...................................................................... 231
Vial Penetration Button............................................................................... 231
Vial Center Adjustment (First) and Last..................................................... 232
Injector Setup Page................................................................................................................ 234
Menu Bar.................................................................................................................. 234
File Menu.................................................................................................................. 235
Done ............................................................................................................ 235
Move To Menu......................................................................................................... 235
All axes home position................................................................................ 235
Single axis Home......................................................................................... 235
Reset Command........................................................................................... 235
Injector Menu ........................................................................................................... 236
Move to stored injector position.................................................................. 236
Auto-search injector height ......................................................................... 236
Store Injector Position................................................................................. 236
Pick a predefined Injector............................................................................ 236
Manual On/Off Menu............................................................................................... 237
Manual On/Off Commands......................................................................... 237
Component parameters Group Box.......................................................................... 237
Injector type................................................................................................. 238
Injection port is enabled check box............................................................. 238
Z tolerance (mm)......................................................................................... 238
Approach speed (mm/s)............................................................................... 238
Position keyboard commands................................................................................... 238
X, Y, Z Axis Frames.................................................................................... 239
Buttons...................................................................................................................... 240
Done ............................................................................................................ 240
Move to stored pos. ..................................................................................... 240
Store Inj. Position........................................................................................ 240
Predefined injector....................................................................................... 240
Contents
Operating Manual 11
Method Selection Page...........................................................................................................241
Select method to edit Group Boxes...........................................................................241
Last loaded...................................................................................................241
New method.................................................................................................241
Load from disk.............................................................................................242
Sampler Configuration Group Box...........................................................................242
Buttons......................................................................................................................242
Ok.................................................................................................................242
Cancel ..........................................................................................................242
Related Topics...........................................................................................................242
TriPlus AS Method Setup Page..............................................................................................243
Menu Bar...................................................................................................................243
File ............................................................................................................................244
New..............................................................................................................244
Load Method................................................................................................244
Save Method ................................................................................................244
Save Method as............................................................................................244
Save Template method.................................................................................244
Print Method................................................................................................245
Exit...............................................................................................................245
Commands ................................................................................................................245
Send Method................................................................................................245
Get Method ..................................................................................................245
Edit............................................................................................................................245
Check method / sampler conf. .....................................................................245
Edit method / sampler conf. Match..............................................................245
Menu Help.................................................................................................................247
Exit Button................................................................................................................247
Related Topics...........................................................................................................247
TriPlus AS Method Setup: General Tag ................................................................................248
Injection Port.............................................................................................................248
Injector.........................................................................................................248
Injection Mode..........................................................................................................249
Mode............................................................................................................249
Sampling ...................................................................................................................251
Sample vol ...................................................................................................251
Plunger strokes.............................................................................................251
Auto air and filling volumes........................................................................251
12 Operating Manual
Contents
Custom air and filling volumes ................................................................... 251
Injection.................................................................................................................... 252
Injection depth............................................................................................. 252
Standard (default value) .............................................................................. 252
Minimum..................................................................................................... 252
Custom......................................................................................................... 252
Pre-injection dwell time (s)......................................................................... 252
Post Injection dwell time (s)........................................................................ 252
Injection depth (mm)................................................................................... 252
Inj speed....................................................................................................... 253
Sampling depth in vial.............................................................................................. 253
Bottom......................................................................................................... 253
Half.............................................................................................................. 253
Custom......................................................................................................... 253
Sampling Vial depth%................................................................................. 254
Sample Viscosity...................................................................................................... 254
Non Viscous ................................................................................................ 254
Viscous........................................................................................................ 254
Custom......................................................................................................... 254
Sample Pull-up speed.................................................................................. 254
Delay after plug strokes (s).......................................................................... 254
Viscosity delay ............................................................................................ 254
TriPlus AS Method Setup: 2nd Inj.Port Tag ......................................................................... 255
2nd Sample mode ..................................................................................................... 255
Injector......................................................................................................... 255
Confirmation................................................................................................ 255
Double-pro................................................................................................... 255
Sample delta ................................................................................................ 255
Delay Inj. 1 to Inj. 2 (s) ............................................................................... 255
Use same Sampling and Inj. Parameters of 1st Injection Port .................... 256
TriPlus AS Method Setup: Washes Tag................................................................................ 257
Washes...................................................................................................................... 257
Single........................................................................................................... 257
Multiple ....................................................................................................... 258
Pre-injection.............................................................................................................. 258
Solvent......................................................................................................... 258
Cycles.......................................................................................................... 258
Solvent volume............................................................................................ 259
Contents
Operating Manual 13
Sample.......................................................................................................................259
Rinses...........................................................................................................259
Rinse volume ...............................................................................................259
Post-Injection............................................................................................................259
Solvent .........................................................................................................259
Cycles...........................................................................................................259
Solvent volume............................................................................................259
TriPlus AS Method Setup: Synch Tag...................................................................................260
GC Synchro start.......................................................................................................260
Standard .......................................................................................................260
Anticipated...................................................................................................260
Delay............................................................................................................260
None.............................................................................................................260
TriPlus AS Method Setup: Synch / Int. Std Tag....................................................................261
GC Synchro start.......................................................................................................262
Standard .......................................................................................................262
Anticipated...................................................................................................262
Delay............................................................................................................262
None.............................................................................................................262
Internal Standard.......................................................................................................262
Int. Std volume.............................................................................................262
Air gap volume ............................................................................................262
Internal standard position.............................................................................262
TriPlus AS Method Setup: Synch / Solvent flush Tag...........................................................264
GC Synchro start.......................................................................................................265
Standard .......................................................................................................265
Anticipated...................................................................................................265
Delay............................................................................................................265
None.............................................................................................................265
Solvent flush .............................................................................................................265
Solvent volume............................................................................................265
Air gap volume ............................................................................................265
Solvent vial..................................................................................................266
Solvent vial deph% ......................................................................................266
TriPlus AS Method Setup: Enrichment Tag ..........................................................................267
Enrichment parameters .............................................................................................267
Enrichment injection repetitions..................................................................267
Time between enrich. Inj. (s).......................................................................267
14 Operating Manual
Contents
TriPlus AS Method Setup: Advanced Tag ............................................................................ 268
Advanced Parameters............................................................................................... 268
Wash solvent depth%.................................................................................. 268
Waste depth%.............................................................................................. 268
Needle speed in vial (mm/s)........................................................................ 269
Solvent filling speed.................................................................................... 269
Bubble elim. Pull-up.................................................................................... 269
Delay between strokes (s)............................................................................ 269
TriPlus AS Method Setup: Cooled/Heated Tray Tag............................................................ 270
Primary/Secondary Tray Temperature ..................................................................... 270
Run Temperature (°C)................................................................................. 270
Stand-By Temperature (°C)......................................................................... 270
TriPlus HS Method Setup Page............................................................................................. 271
Menu Bar.................................................................................................................. 272
File Menu.................................................................................................................. 272
New.............................................................................................................. 272
Load Method ............................................................................................... 272
Save Method................................................................................................ 272
Save Method as............................................................................................ 272
Save Template method................................................................................ 273
Print Method................................................................................................ 273
Exit .............................................................................................................. 273
Menu Commands...................................................................................................... 273
Send Method................................................................................................ 273
Get Method.................................................................................................. 273
Menu Edit................................................................................................................. 273
Check method / sampler conf...................................................................... 273
Edit method / sampler conf. Match ............................................................. 273
Menu Help................................................................................................................ 275
Exit Button................................................................................................................ 275
Related Topics.......................................................................................................... 275
TriPlus HS Method Setup: General Tag................................................................................ 276
Injection Port ............................................................................................................ 276
Injector......................................................................................................... 276
Mode............................................................................................................ 277
Incubation Mode.......................................................................................... 277
Analysis time............................................................................................................ 277
Analysis time (min)..................................................................................... 277
Contents
Operating Manual 15
Incubation..................................................................................................................278
Agitator temperature (°C)............................................................................278
Incubation Time (min).................................................................................278
Progressive incubation time (min)...............................................................278
Multiple extraction venting time (s) ............................................................278
Agitator on (s)..............................................................................................278
Agitator off (s) .............................................................................................278
Sample.......................................................................................................................279
Sample Draw (ml)........................................................................................279
Enrichment counts (#)..................................................................................279
Enrichment delay (min) ...............................................................................279
Sampling depth in vial ..............................................................................................279
Standard .......................................................................................................279
Custom.........................................................................................................279
Sampling vial depth (mm) ...........................................................................279
Double Pro 2nd injector............................................................................................280
Injector.........................................................................................................280
Sample delta.................................................................................................280
Delay Inj. 1 to Inj. 2 (s)................................................................................280
TriPlus HS Method Setup: Syringe Tag.................................................................................281
Syringe......................................................................................................................281
Syringe temperature (°C).............................................................................281
Enable Pre-filling.........................................................................................282
Filling volume (ml)......................................................................................282
Filling count (#)...........................................................................................282
Filling delay (s)............................................................................................282
Pre-Inj. Syringe flush (fixed 5 seconds) ......................................................282
Post injection syringe flush (sec).................................................................282
Speed.........................................................................................................................282
Filling speed (ml/min)..................................................................................283
Injection (ml/min)........................................................................................283
Injection ....................................................................................................................283
Injection Depth (mm)...................................................................................283
Pre-Injection delay (s)..................................................................................283
Post-Injection Delay.....................................................................................283
TriPlus HS Method Setup: Syringe Solvent Washes Tag......................................................284
Washes......................................................................................................................284
Single ...........................................................................................................285
16 Operating Manual
Contents
Multiple ....................................................................................................... 285
Clean............................................................................................................ 285
Solvent......................................................................................................... 285
Dry time (min)............................................................................................. 285
Wash frequency........................................................................................... 285
TriPlus HS Method Setup: Synch / St-by Tag....................................................................... 286
St-by temperature ..................................................................................................... 286
Syringe temperature (°C)............................................................................. 286
Agitator temperature (°C)............................................................................ 287
St-by Syringe flush................................................................................................... 287
Syringe flush................................................................................................ 287
GC Synch start mode................................................................................................ 287
Normal......................................................................................................... 287
Anticipated .................................................................................................. 287
Anticipated sync before incubation end ................................................................... 287
Anticipated time (min) ................................................................................ 287
TriPlus HS Method Setup: Advanced Tag ............................................................................ 288
Advanced Parameters............................................................................................... 288
Needle speed in vial (mm/s)........................................................................ 288
TriPlus SPME Method Setup Page........................................................................................ 289
Menu Bar.................................................................................................................. 289
File Menu.................................................................................................................. 289
New.............................................................................................................. 290
Load Method ............................................................................................... 290
Save Method................................................................................................ 290
Save Method as............................................................................................ 290
Save Template method................................................................................ 290
Print Method................................................................................................ 290
Exit .............................................................................................................. 290
Menu Commands...................................................................................................... 291
Send Method................................................................................................ 291
Get Method.................................................................................................. 291
Menu Edit................................................................................................................. 291
Check method / sampler conf...................................................................... 291
Edit method / sampler conf. Match ............................................................. 291
Menu Help................................................................................................................ 293
Exit Button................................................................................................................ 293
Related Topics.......................................................................................................... 293
Contents
Operating Manual 17
TriPlus SPME Method Setup: Parameters Page ....................................................................294
Desorb Port ...............................................................................................................294
Injector.........................................................................................................294
Mode .........................................................................................................................295
Incubation Mode..........................................................................................295
Sample Vial Parameters............................................................................................295
Needle speed in vial.....................................................................................295
Extract time..................................................................................................295
Incubation..................................................................................................................295
Agitator st-by temperature (°C)...................................................................296
Incubation Time...........................................................................................296
Progressive incubation time (min)...............................................................296
Agitator on...................................................................................................296
Agitator off...................................................................................................296
Sampling Vial Depth.................................................................................................296
Sampling Depth Mode.................................................................................296
Sampling vial depth .....................................................................................297
Injection ....................................................................................................................297
Injector Depth (mm) ....................................................................................297
Desorb time (min)........................................................................................297
Analysis Time...........................................................................................................297
Analysis time (min)...................................................................................................297
GC Synch Start Mode...............................................................................................297
Start mode....................................................................................................297
TriPlus SPME Method Setup:Fiber Conditioning Page.........................................................298
Internal Standard.......................................................................................................298
Internal Standard vial...................................................................................298
Int. Standard Ads. time (min) ......................................................................298
Conditioning Port......................................................................................................298
Port ID..........................................................................................................298
Desorb time..................................................................................................298
Fiber Conditioning Station........................................................................................299
Conditioning temperature (°C) ....................................................................299
St-by temperature (°C).................................................................................299
Chapter 6
Operations.......................................................................................................................................... 301
Overview................................................................................................................................302
18 Operating Manual
Contents
Instrument Power On................................................................................................ 302
Instrument Configuration ......................................................................................... 302
Sampler Set-up ......................................................................................................... 302
Injector Set-up .......................................................................................................... 302
Method Editing......................................................................................................... 303
Template Method......................................................................................... 303
How to Create / Load a Method.................................................................. 303
Template Method Summary..................................................................................... 304
AS Template Methods................................................................................. 305
HS Template Method .................................................................................. 307
Start Analysis......................................................................................................................... 310
Sampler Movements.............................................................................................................. 311
Basic Single Injector................................................................................................. 311
Internal Standard Post Single Injector...................................................................... 313
Needle Solvent Wash Single Injector....................................................................... 315
Basic Confirmation................................................................................................... 317
Basic Double Pro...................................................................................................... 320
Chapter 7
Maintenance and Troubleshooting ...................................................................................................323
Maintenance........................................................................................................................... 324
Current Maintenance ................................................................................................ 324
Reinstallation of the Injection Device on the Sliding Plate......................... 337
Messages................................................................................................................................ 345
Status Messages........................................................................................................ 345
Error Messages......................................................................................................... 347
Alarm Messages ....................................................................................................... 350
Main Alarm Messages................................................................................. 350
Boot Alarm Messages.................................................................................. 351
Safety Cut Off........................................................................................................................ 352
Chapter 8
LAN Set-up..........................................................................................................................................353
Introduction............................................................................................................................ 354
IP Address and LAN Communication Port........................................................................... 354
Network Cables ..................................................................................................................... 355
Set-Up.................................................................................................................................... 356
NE-4110S Series LAN Module................................................................................ 356
Contents
Operating Manual 19
Reset Button.................................................................................................356
DE-311M Series LAN Module.................................................................................356
Reset Button.................................................................................................356
Chapter 9
TriPlus Control from the Pocket PC................................................................................................. 377
Pocket PC Connection............................................................................................................378
Materials Required....................................................................................................378
TriPlus Software Installation ....................................................................................379
Connection Options...................................................................................................380
Connection Via Serial Port ..........................................................................381
Connection Via Infrared Transceiver...........................................................382
Connection Via Wireless Network ..............................................................382
Connection Via Ethernet Card.....................................................................382
Connect the Pocket PC via Network.........................................................................383
Configuration of the TriPlus Software......................................................................386
User Interface.........................................................................................................................390
Launch the TriPlus Software.....................................................................................390
Initial Page .............................................................................................................................391
Initial Page Overview................................................................................................391
File Menu..................................................................................................................392
Commands Menu......................................................................................................393
Configuration Page.................................................................................................................395
Sampler Setup Page................................................................................................................397
Component Information Page................................................................................................399
Goto Commands .......................................................................................................401
Vial Penetration.........................................................................................................402
Vial #1 Adjustment...................................................................................................402
Injector Setup Page ................................................................................................................403
Method Selection Page...........................................................................................................409
TriPlus AS Method Setup Page..............................................................................................410
TriPlus AS Method Setup Page Description.............................................................411
Configuration Mismatch Page ..................................................................................413
TriPlus AS Method Setup: General Tag...................................................................415
TriPlus AS Method Setup: Washes Tag ...................................................................419
TriPlus AS Method Setup: Synch. Tag.....................................................................421
TriPlus AS Method Setup: Synch / Int.Std Tag........................................................422
TriPlus AS Method Setup: Synch / Solvent Flush Tag.............................................424
20 Operating Manual
Contents
TriPlus AS Method Setup: 2nd Inj. Port Tag............................................................ 426
TriPlus AS Method Setup: Enrichment Tag............................................................. 427
TriPlus AS Method Setup: Advanced Tag............................................................... 428
TriPlus HS Method Setup Page............................................................................................. 429
TriPlus HS Method Setup Page Description ............................................................ 430
Configuration Mismatch Page.................................................................................. 432
TriPlus HS Method Setup: General Tag................................................................... 434
TriPlus HS Method Setup: Syringe Tag................................................................... 437
TriPlus HS Method Setup: Syringe Solvent Wash Tag............................................ 439
TriPlus HS Method Setup: Synch / St-by Tag.......................................................... 440
TriPlus HS Method Setup: Advanced Tag............................................................... 441
Appendix A
TriPlus Sampler for Multiple GC Configuration ..............................................................................443
Appendix B
Customer Communication ...............................................................................................................449
How To Contact Us...............................................................................................................449
Reader Survey........................................................................................................... 450
Glossary.............................................................................................................................................. 451
Index.................................................................................................................................................... 457
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Thermo Fisher Scientific TriPlus Automatic Sampling System Operating instructions

Type
Operating instructions

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