Varian GC 3800 Assembly Procedures

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PARTS

LIST

DOC: 03-925914-01/02

DESC: Micro - TCD Installation

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TOOLS

PREPARED BY: Sax Makthepharack REVISED BY:

CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN

-

03 - 10 - 00

Michael Slaughter

MENU

CHG

HISTORY

INSTALLATION OF MICRO-TCD

STATION #3, ASSEMBLY PROCEDURES

ADAPTER (SEE NEXT PAGE)

TEE (SEE NEXT PAGE)

PARTS

LIST

DOC: 03-925914-01/02

DESC: Micro - TCD Installation

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PREPARED BY: Sax Makthepharack REVISED BY:

CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN

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03 - 10 - 00

Michael Slaughter

MENU

CHG

HISTORY

EFC CARRIER

INJECTOR (REF.)

SEE DETAIL “A”

ANALYTICAL COLUMN (CP-7758)

REFERENCE COLUMN (CP-735732)

SEE DETAIL “B”

03-925910-01

BALANCE ADAPTOR

SEE DETAIL “B”

SCHEMATIC OF MICRO-TCD WITH ADAPTOR REFERENCE

DETAIL “A” DETAIL “B”

INJECTOR (REF.)

CLICK HERE FOR

MICRO-TCD ASSEMBLY

16-000589-00

TEE

28-694581-00

FERRULE

03-949551-00

NUT

CP-470100

FERRULE, Ø0.32 COLUMN

CP-085887

NUT

(03-925916-01)

MICRO-TCD REF. SIDE, ADAPTOR FACTORY

MICRO-TCD CELL (REF.)

SCHEMATIC OF MICRO-TCD WITH INJECTOR REFERENCE

PARTS

LIST

DOC: 03-925914-01/02

DESC: Micro - TCD Installation

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PREPARED BY: Sax Makthepharack REVISED BY:

CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN

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03 - 10 - 00

Michael Slaughter

MENU

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HISTORY

INSTALLATION OF MICRO-TCD:

1. ENSURE GC OVEN INSULATION IS CAREFULLY WRAPPED UNDER AND

AROUND, THE MICRO-TCD TO PREVENT COLUMN OVEN CONDITIONS

COUPLING WITH DETECTOR.

2. FEED HEATER AND PROBE TO LOCATION ON PWA’S

- HEATER TO ZONE ON POWER PWA.

- PROBE TO ZONE ON MAIN PWA.

3. INSTALL MICRO-TCD PWA BOARD (03-925904-01) AND SECURE. ROUTE FLAT,

RIBBON CABLE FROM MICRO-TCD ALONGSIDE PNEUMATICS BULKHEAD AND

AROUND TO MICRO-TCD PWA BOARD. SECURE WITH CABLE CLAMP.

03-925904-01

MICRO-TCD PWA

HEATER CONNECTOR ZONE

PROBE CONNECTOR ZONE

03-925914-11/12

MICRO-TCD SUB-ASSEMBLY

PARTS

LIST

DOC: 03-925914-01/02

DESC: Micro - TCD Installation

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PREPARED BY: Sax Makthepharack REVISED BY:

CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN

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03 - 10 - 00

Michael Slaughter

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HISTORY

PARTS

LIST

DOC: 03-925862-00

DESC:

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3800GC W/DEFC Leak Test Procedure

1

TOOLS

PREPARED BY: Sax Makthepharack REVISED BY:

CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN

-

06 - 09 - 98

Michael Slaughter

MENU

CHG

HISTORY

INJECTOR EFC LEAK TEST PROCEDURE

1. Install ETS software Version 1.6.2 or newer. (be sure to discharge yourself before touching ROM pwa.)

2. Set the DIP Switches on the main board as shown:

3. Turn on power and connect Carrier Gas inlet tube.

4. Make sure jumpers on EFC board are in the correct position.

5. Cap off all unused gas inlet fittings and the Injector column out fitting.

6. Press MENU key.

7. Check com board if installed (under AOC cont.) pg.2.

8. Check Detector Electrometer pwa’s, (3) are they present?.

9. Check EFC’s, (5) are they present? Are they good?

10. If EFC’s are present and good, press Enter Key and set to Pressure DAC 5.00 and Flow DAC to 3.00.(Left blue toggle key below display 3

times to pressure up instrument).

11. After completing items 1 thru 10, turn on Carrier Gas.

12. When the pressure is stable, turn OFF Carrier Gas and press LEAKSTOP Key. (blue key below display)

13. The leak test procedure will run for 5 minutes then stop and display the leak value for the 5 min. period. (< .30 + .10 for each EFC installed is

the acceptance criteria, (if the test fails, retest and measure the flow at the EFC Vent tube. If a leak is detected and is less than .10 ml/min.

subtract the amount from your total leak value. If that value is less than the spec (above), the instrument passed the test. If over, the

instrument Fail and the leak must be found and corrected. Retest as above until a pass condition is reached.

14. Record the resulting value of the leak test on the QC Record Sheet.

15. Press Menu Key, go to TEMPERATURE MENU (4) check and press Enter.

16. Set all Temp zones to NOT USED and press Enter. (use decrease key)

17. Go to Pg.2 of 3, check Vent Doors for unrestricted opening and closing. (toggle ON enter, OFF enter)

18. If any Cryo is installed, go to pg. 3. Select the proper external event then activate to assure opening and closing. (blue Time Off/On key

under display)

19. Go back to pg. 1 and Enable those zones used. Observe temperature go to 50 deg. and hold stable.

20. Press CONTACTOR key.

21. If Fan is running, go back to pg. 2 and turn off Fan.

22. Go to EFC Control (5) enter, select flow key and measure each Inj/Det. for some amount of flow.

23. Go to Main Menu, select EFC Control, press enter, go to EFC location (front, middle, rear) then go to pg. 6. In lower right corner of display

see EFC type, is it correct? (type 1,3,4,5, etc.) Turn Instrument Off, replace ROM board and restart instrument. Initial Display should

appear.

PARTS

LIST

DOC: 03-925862-00

DESC:

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3800GC W/DEFC Leak Test Procedure

1

TOOLS

PREPARED BY: Sax Makthepharack REVISED BY:

CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN

-

06 - 09 - 98

Michael Slaughter

MENU

CHG

HISTORY

DETECTOR EFC LEAK TEST PROCEDURE

1. Connect Helium to makeup line for FID, TSD, ECD and TCD. Connect Helium to H2 line for PFPD and TCD(H2).

2. Cap off all other gas inlets

3. Make sure DEFC position jumpers in correct position.

4. Cap all other inlets (Top and bottom of Detector)

5. Plug in customer software.

6. Turn on the power

7. Press ∞ to go to local mode.

8. From the “Instrument Setup” menu, Enter the IEFC type(s) in the appropriate positions in the “Heated Zones” screen

9. Save and Exit

10. When the GC is done initializing (~2 minutes), Press ∞ to go to local mode.

11. Press “Detector” button to get to the Detector Menu

12. For each detector:

* Pick Detector

* Go to the “adjustments” screen, page 2

* Turn on the gas

* Within 2 minutes, the flowrate of the Helium channel (1) should go to 0. In the case of PFPD, channel 2 is used. In the case of

TCD(H2), Channel 1 is used.

* If flowrate does not go to 0, fix leaks and retest. (.1 is acceptable for PFPD with manufacture engineer approval).

* Turn off gas and GC

PARTS

LIST

DOC: 03-925709-01

DESC: Assy, Column Oven Cryogenics, (CO2)

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HISTORY

TOOLS

PREPARED BY: Sax Makthepharack REVISED BY:

CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN

-

04 - 05 - 00

Michael Slaughter

MENU

ASSY, COLUMN OVEN CRYOGENICS, (CO2)

3800GC SUB-ASSEMBLIES STATION, ASSEMBLY PROCEDURES

PARTS

LIST

DOC: 03-925709-01

DESC: Assy, Column Oven Cryogenics, (CO2)

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TOOLS

PREPARED BY: Sax Makthepharack REVISED BY:

CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN

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04 - 05 - 00

Michael Slaughter

MENU

NOTES:

1.

03-925567-01

3800 CO2 VALVE FACTORY INSTALL

COLUMN OVEN CRYOGENICS EXPLODED VIEW

28-694205-00

1/8IN ADAPTER

28-609966-00

ADAP, COMP., 1/8 X 1/8 SST

12-222060-04, 2 PLCS

SCREW, 10-32 X 1/4 PAN, SS

03-925261-01

BRACKET, CRYO VALVE

03-925497-01

CO2 OUTLET TUBE

FLOW DIRECTIOIN

60° (REF.)

INSTALL TEFLON TAPE ON FITTING THREADS AS REQUIRE AND

FRONT VIEW (REF.)

1

2

CO2 OUTLET TUBE (REF.)

3800 CO2 VALVE

FACTORY INSTALL

CRYO VALVE BRACKET (REF.)

1-1/2 - 2 TURNS IN THE DIRECTION OF THREADS.

SURE TUBING TOWARD THE FAN SHAFT INSIDE THE OVEN

WHEN INSTALLING THE CO2 OUTLET TUBE (03-925497-01) MAKE2.

PARTS

LIST

DOC: 03-925709-01

DESC: Assy, Column Oven Cryogenics, (CO2)

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HISTORY

TOOLS

PREPARED BY: Sax Makthepharack REVISED BY:

CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN

-

04 - 05 - 00

Michael Slaughter

MENU

COLUMN OVEN

CRYOGENICS ASSEMBLY (REF.)

22-799995-00

BUSHING, STRAIN REL.

12-901163-00, 2 PLCS

SCREW, 8-32 X 3/8 SEM

03-925489-01

ASSY, CABLE, CRYO EXTENSION

9

1

7

NOTE:

CONNECT CRYOU EXTENSIO

WIRES PIN TO (J-47) ON PWA

(J-47)

CONNECTOR (REF.)

PARTS

LIST

DOC: 03-925709-01

DESC: Assy, Column Oven Cryogenics, (CO2)

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HISTORY

TOOLS

PREPARED BY: Sax Makthepharack REVISED BY:

CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN

-

04 - 05 - 00

Michael Slaughter

MENU

PARTS

LIST

DOC: 03-925708-01

DESC: Assy, Column Oven Cryogenics

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HISTORY

TOOLS

PREPARED BY: Sax Makthepharack REVISED BY:

CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN

-

04 - 25 - 00

Micheal Slaughter

MENU

ASSY, COLUMN OVEN CRYOGENICS (LN2 VERSION)

3800GC STATION #3, ASSEMBLY PROCEDURES

PARTS

LIST

DOC: 03-925708-01

DESC: Assy, Column Oven Cryogenics

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HISTORY

TOOLS

PREPARED BY: Sax Makthepharack REVISED BY:

CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN

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04 - 25 - 00

Micheal Slaughter

MENU

03-925557-01

3800 LN2 VALVE

03-925261-01

BRACKET, CRYO VALVE

28-691979-00

1/4 T X 1/8 P BR MALE CONN.

28-695130-00

B-4-TA-1-2 ADAPTER, COMPRESSION 1/4 TUBE

03-925378-01

LIQUID NITROGEN OUTLET TUBE

03-925489-01

ASSY, CABLE, CRYO EXTENSION

14-312010-00, 2 PLCS

WASHER, EXT LOCK, #10

OUTLET SIDE

INLET SIDE

NOTES:

1

12-222010-06, 2 PLCS

10-24 X 3/8 PH PAN

INSTALL TEFLON PIPE TAPE (88-189669-00) FITTING THREADS PRIOR TO INSTALLATION.

2 WHEN INSTALLING LIQUID NITROGEN OUTLET TUBE (03-925378-01) INTO THE 1/4 T X 1/8 P

BR MALE CONNECTOR (28-691979-00), MAKE SURE HOLES ON THE END OF OUTLET TUBE

IS UPWARD PRIOR TO TIGHTENING. SEE DETAIL “A”.

2

1

OUTLET TUBING (REF.)

SEE NOTE #2

FOR REFERENCE ONLY

REFER TO NEXT PAGE FOR CONFIGURATION

PARTS

LIST

DOC: 03-925708-01

DESC: Assy, Column Oven Cryogenics

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HISTORY

TOOLS

PREPARED BY: Sax Makthepharack REVISED BY:

CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN

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04 - 25 - 00

Micheal Slaughter

MENU

LN2 OVEN CRYO

NO OVEN CRYO

BULK ISSUE ITEMS (03-925515-XX)

3 INJECTORS 2 INJECTORS 1 INJECTOR NO INJECTOR

57-000235-00

PRESSURE RELIEF VALVE

1

28-695036-00

SWAGELOK #B-4-TA-7-4

28-691946-00

TEE, UNION 1/4” TUBE BRASS

1

03-925651-01

TUBE, 1/4” CROSS, TEE, CONNECTOR

03-925654-01

DEFLECTOR, AIR FLOW

PARTS

LIST

DOC: 03-925708-01

DESC: Assy, Column Oven Cryogenics

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HISTORY

TOOLS

PREPARED BY: Sax Makthepharack REVISED BY:

CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN

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04 - 25 - 00

Micheal Slaughter

MENU

VALVE ARRANGEMENT (REF.)

23-230938-00

COVER, SQUARE

88-494510-00, 5” LG

PIPE INSULATION 3/8” ID .42”

12-901163-00, 2 PLCS

SCREW, 8-32 X 3/8, SEM

PARTS

LIST

DOC: 03-925632,633,634&635-XX

Assy, 1177 Manual and Type 5 EFC Installation

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HISTORY

TOOLS

PREPARED BY: Sax Makthepharack REVISED BY:

CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN

-

12 - 03 - 99

Steve Swihart

MENU

DESC:

ASSY, 1177 MANUAL AND TYPE 5 EFC INSTALLATION

3800GC STATION #3, ASSEMBLY PROCEDURES

PARTS

LIST

DOC: 03-925632,633,634&635-XX

Assy, 1177 Manual and Type 5 EFC Installation

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TOOLS

PREPARED BY: Sax Makthepharack REVISED BY:

CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN

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12 - 03 - 99

Steve Swihart

MENU

DESC:

03-925469-01

BRACKET, SPLIT VLV. MTG.

27-239921-00

GAGE PRESSURE, 0-60 PSI

28-694302-00

ADAPTER 1/8” UNION

BRS. COMP. FTG.

03-918853-03

PEEK TUBING, GREEN

27-180135-00

KOJIMA FLOW CONTL.

03-918959-02

PENCIL FILTER

03-925467-01

SOLENOID VALVE 3- WAY

03-918174-00

BACK PRESSURE REGULATOR

03-918853-03

PEEK TUBING, GREEN

03-918853-03

PEEK TUBING, GREEN

28-158923-00

TYGON TUBING, CLEAR.

FROM INJECTOR

VENT

28-691944-00

TEE, 1/16” BRASS

03-918853-03

PEEK TUBING, GREEN

12-222008-04

SCREW, 8-32,X 1/4” LG PH,

SST 2EA

03-918853-07

PEEK TUBING, NATURAL

03-918853-03

PEEK TUBING, GREEN

CLICK HERE

TO SEE SOLENOID

CONNECTION TO J42

ON POWER BD.

03-917157-00

WASHER , VITON FERRLE 3EA

03-917084-00

NUT, VITON FERRULE 3EA

03-917142-00

VITON FERRLE 3EA

03-917157-00

WASHER , VITON

FERRLE 2EA

03-917142-00

VITON FERRLE 2EA

SEE ADJ.

NOTE/ DETAIL

03-917084-00

NUT, VITON FERRULE 2EA

03-917157-00

WASHER , VITON FERRLE 2EA

03-917142-00

VITON FERRLE 2EA

03-917084-00

NUT, VITON FERRULE

3EA

03-917157-00

WASHER , VITON FERRLE

3EA

03-917142-00

VITON FERRLE 3EA

12-901132-00

SCREW 8-32 X 3/8” LG EXT STL. 2EA

03-918853-03

PEEK TUBING, GREEN

03-917128-00

NUT, 1/6 NPS-”O” RING

“CARRIER GAS IN”

03-917157-00

WASHER , VITON FERRLE

03-917084-00

NUT, VITON FERRULE

03-917142-00

VITON FERRLE

28-849067-00

10-32 ADAPTER HOSE

03-918853-07

PEEK TUBING 1/8” NAT.

03-918853-07

PEEK TUBING 1/8” NAT.

28-849067-01

BESWICK FITTING

NOTE: DETAIL OF SOLENOID VALVE

12-901162-00

SCREW (2 PL)

PARTS

LIST

DOC: 03-925632,633,634&635-XX

Assy, 1177 Manual and Type 5 EFC Installation

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HISTORY

TOOLS

PREPARED BY: Sax Makthepharack REVISED BY:

CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN

-

12 - 03 - 99

Steve Swihart

MENU

DESC:

03-925996-XX

1177 INJECTOR, EFC

03-925110-01

EFC TYPE 1

12-901163-00

SCREW, 8-32 X 3/8” EXT.

4 ON EFC, 2 INJ., 6 TOTAL

03-925374-01

TEMPERATURE PROBE

03-925987-01

120V HTR. CART., 100V

03-925987-02

220V HTR. CART., 100V

03-925987-03

101V HTR.CART., 100V

03-918532-01

VAR SEPTUM PURGE

NOTE:

1 BE SURE INJ. IS IN ONE OF THE (4) A/S LOCATIONS. SEE INJ. COVER

FOR ALIGNMENT.

1

PARTS

LIST

DOC: 03-925632,633,634&635-XX

Assy, 1177 Manual and Type 5 EFC Installation

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HISTORY

TOOLS

PREPARED BY: Sax Makthepharack REVISED BY:

CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN

-

12 - 03 - 99

Steve Swihart

MENU

DESC:

1177 INJECTOR

EFC TYPE 5

CLICK HERE OR ON PICTURE

TO SEE S/A EXPLOSION

CLICK HERE OR ON PICTURE

TO SEE S/A EXPLOSION

INJ

FRONT

DET.

FRONT

INJ

MIDDLE

DET.

MIDDLE

INJ

REAR

DET.

REAR

INJECTOR

SPLIT VENT

SPARE

INJECTOR SIDE MANIFOLD PLUMBING

G.C. FRONT

G.C. BACK

VENT THRU

PNEU. PANEL

SPLIT

VENT

PRESSURE

SENSE (TO 1177)

CARRIER IN FROM

CROSS FITTING

CARRIER

OUT

CARRIER IN - FROM EFC

CARRIER IN

(GREEN)

(GREEN COLORED MARKER)

SPLIT VENT

SEPTUM PURGE

TO SPORT VALVE

(NO COLORED MARKER)

PARTS

LIST

DOC: 03-925630&631-XX

DESC: Assy, 1177 EFC Injector Installation

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HISTORY

TOOLS

PREPARED BY: Sax Makthepharack REVISED BY:

CONTROL: INDUSTRIAL ENGINEERING REV. DATE: SHOWN

-

12 - 1 - 99

Steve Swihart

MENU

ASSY, 1177 EFC INJECTOR INSTALLATION

3800GC STATION #3, ASSEMBLY PROCEDURES

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Varian GC 3800 Assembly Procedures

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