M
ODEL
951C
NO
X
A
NALYZER
748214-N
Rosemount Analytical
ii
September 1997
S
ECTION
3. I
NITIAL
S
TARTUP AND OPERATION
3.1 FRONT PANEL INDICATORS AND CONTROLS.....................................3-1
3.1.1 Display ......................................................................................3-1
3.1.2 Range Selection.........................................................................3-1
3.1.3 Sample Pressure Gauge............................................................3-2
3.1.4 Ozone Pressure..........................................................................3-2
3.1.5 Zero and Span Potentiometers...................................................3-2
3.1.6 Ozone Interlock ..........................................................................3-2
3.2 STARTUP PROCEDURE.........................................................................3-2
3.3 CALIBRATION .........................................................................................3-4
3.3.1 Zero Calibration..........................................................................3-4
3.3.2 Upscale Calibration ....................................................................3-4
3.4 ROUTINE OPERATION...........................................................................3-5
3.5 CONVERTER TEMPERATURE ADJUSTMENT PROCEDURE..............3-5
3.6 MEASUREMENT OF CONVERTER EFFICIENCY..................................3-7
3.7 RECOMMENDED CALIBRATION FREQUENCY....................................3-8
S
ECTION
4. T
HEORY
4.1 NITRIC OXIDE DETERMINATION BY CHEMILUMINESCENCE
METHOD ......................................................................................4-1
4.2 ANALYZER FLOW SYSTEM....................................................................4-1
4.2.1 Flow of Sample, Standard Gas or Zero Gas to
Reaction Chamber........................................................4-1
4.2.2 Ozone Generation......................................................................4-2
4.3 SIGNAL PROCESSING ELECTRONICS SYSTEM.................................4-2
4.4 ANALYZER THERMAL SYSTEM.............................................................4-3
S
ECTION
5. R
OUTINE SERVICING
5.1 SYSTEM CHECKS AND ADJUSTMENTS................................................5-1
5.1.1 Display Fullscale Span Adjustment ............................................5-1
5.1.2 Overall Sensitivity.......................................................................5-2
5.1.3 Ozone Output.............................................................................5-2
5.1.4 Background Current ...................................................................5-3
5.1.5 Excessive Photomultiplier Dark Current .....................................5-3
5.2 SERVICING FLOW SYSTEM ..................................................................5-3
5.2.1 Cleaning Sample Capillary .........................................................5-3
5.2.2 Ozone Restrictor Fitting..............................................................5-4
5.3 PHOTOMULTIPLIER TUBE/REACTION CHAMBER ..............................5-5