Thermo Fisher Scientific iTEVA Software Owner's manual

iTEVA Software Manual

Operators Manual

8499 400 30001

190809

SOLAAR House, 19 Mercers Row, Cambridge CB5 8BZ.United Kingdom.

Telephone +44 (0) 1223 347400, Fax +44 (0) 1223 347402.

www.thermoﬁsher.com

Thermo ScientiﬁciTEVA Software Manual

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Thermo Scientiﬁc iTEVA Software Manual i

Contents

Chapter 1 Introduction .................................................................................................1-1

iTEVA Security ..................... ......................................................1-3

Opening the Program ..................................................................1-5

ITEVA Security Login ........................................................................1-5

Conventions ................................................................................1-6

Chapter 2 iTEVA Control Center ................................................................................. 2-1

iTEVA Control Center ......................................................................2-3

e Menu Bar .............................................................................2-4

File ..............................................................................................2-4

File, Log On ................................................................................2-4

File, Log O ................................................................................2-4

File, Print Journal ........................................................................2-5

File, Journal Print Preview ...........................................................2-5

File, Print Setup ..........................................................................2-5

File, Page Setup ...........................................................................2-5

File, Exit ......................................................................................2-6

View ..............................................................................................2-6

Tools, Options ..................................................................................2-6

Tools, Options, General ..............................................................2-7

Tools, Options, Periodic Table .....................................................2-7

Tools, Options, Journal ...............................................................2-8

Tools, Options, Directories .......................................................2-10

Tools, Options, Print Options ...................................................2-11

Tools, Options, Analyst .............................................................2-12

iTEVA Security ..................... ....................................................2-12

Tools, Options, New Method Parameters ..................................2-12

Tools/Options/Access Rights - only for iTEVA Security .............2-13

iTEVA SQL Databases ..............................................................2-17

iTEVA Security ..................... ....................................................2-17

Tools, Options, Application Database .......................................2-18

Database Wizard .............................................................................2-18

Database Info ............................................................................2-20

Create .......................................................................................2-20

Detach ......................................................................................2-20

Attach .......................................................................................2-20

Backup ......................................................................................2-21

Restore ......................................................................................2-21

Users (only for iTEVA, not present for iTEVA Security) ............2-21

Create New Database ................................................................2-21

Add a New Connection .............................................................2-23

Copy Methods/Results ..............................................................2-25

Change Active Connection ........................................................2-25

Thermo Scientiﬁcii iTEVA Software Manual

Deleting/Exporting/Importing Databases ........................................2-25

Deleting a Database ........................................................................2-25

Editing/Deleting a Connection .................................................2-26

Exporting/Importing a Database from/to another iCAP ...........2-26

Database Upgrades ....................................................................2-26

Tools, Instrument Options ..............................................................2-27

Autosampler ..............................................................................2-27

Sample Introduction .................................................................2-27

Enable Drain Sensor ..................................................................2-28

Accessory ...................................................................................2-28

Help ............................................................................................2-28

Help, Help Topics .....................................................................2-28

Feature request / Incident form .................................................2-28

Help, About iTEVA ..................................................................2-30

e Tool Bar....................................................................................2-31

e Workspace ..........................................................................2-31

e Journal ...............................................................................2-32

e Status Bar ...........................................................................2-33

New Firmware dialog box ..........................................................2-34

Chapter 3 Analyst ......................................................................................................... 3-1

Analyst Window ................................................................................3-3

Chapter 4 Analyst, Method ......................................................................................... 4-1

Analyst, Method ................................................................................4-3

Method Menu Bar.......................................................................4-3

Method .......................................................................................4-3

Create a new Method ........................................................................4-4

Periodic Table, Map Editor ..............................................................4-10

Status ............................................................................................4-12

Analysis Preferences .........................................................................4-13

Sample Options ........................................................................4-14

Source .......................................................................................4-14

Analysis Maximum Integration Times .......................................4-15

Calibration Mode ............................................................................4-16

Trailing Fullframe Options ..............................................................4-18

Automated Output ..........................................................................4-21

Automated Output, Unknowns .................................................4-21

Automated Output, Standards ..................................................4-23

Report Preferences ...........................................................................4-24

Report Preferences, Unknowns ..................................................4-24

Checks. ...........................................................................................4-28

Check Type, QC .......................................................................4-31

Check Type, Recovery ...............................................................4-33

Check Type, Limit Check ..........................................................4-34

Check Type, Duplicate ..............................................................4-35

Sequence Automation .....................................................................4-35

Initial Actions ............................................................................4-37

Contents

Thermo Scientiﬁc iTEVA Software Manual iii

Continuing Actions ...................................................................4-38

End Actions ..............................................................................4-40

Global QC Properties ......................................................................4-40

Continuing Actions, Failure options ................................................4-42

Autosampler ....................................................................................4-42

Source Settings ................................................................................4-45

Internal Standards ...........................................................................4-50

Selecting Internal Standards ......................................................4-51

Standards ..................................................................................4-53

Elements .........................................................................................4-56

Elements, General .....................................................................4-57

Elements, Standards ..................................................................4-60

Elements, Fit .............................................................................4-63

Elements, IEC ...........................................................................4-75

Elements, Subarray ....................................................................4-77

Method Reports ..............................................................................4-80

Method, Open ..........................................................................4-81

iTEVA Security ................................................................................4-85

Select a Method, Sign and Audit Trail .............................................4-85

iTEVA Security ................................................................................4-89

Method, Sign Method .....................................................................4-89

Method, Audit Trail ..................................................................4-90

Toolbar ............................................................................................4-90

Tools ............................................................................................4-92

View ............................................................................................4-94

Help ............................................................................................4-95

Chapter 5 Analyst, Analysis ....................................................................................... 5-1

Analyst, Analysis................................................................................5-3

Tool Bar ......................................................................................5-3

Method .......................................................................................5-6

iTEVA Security .................................................................................5-7

Run ..............................................................................................5-8

Run Full Frame ...........................................................................5-8

Time Scan .................................................................................5-16

Run, Unknown, QC, Standard, Blank.............................................5-22

Calibration ................................................................................5-27

Active Method, Workspace ..............................................................5-30

Results ............................................................................................5-43

Instrument ......................................................................................5-54

Tools ............................................................................................5-60

View ............................................................................................5-67

Help ............................................................................................5-69

Chapter 6 Analyst, Sequence ..................................................................................... 6-1

Analyst, Sequence ..............................................................................6-3

Sequence Menu Bar .....................................................................6-3

Contents

Thermo Scientiﬁciv iTEVA Software Manual

Auto Session ................................................................................6-4

Auto-Session,New Autosampler ...................................................6-4

Auto-Session, New Manual .........................................................6-7

Run Auto-Session ......................................................................6-10

Autosampler Error messages ......................................................6-11

Signing Autosessions and Autosession Audit Trail ............................6-13

Sequence .........................................................................................6-14

Sequence Tool Bar .....................................................................6-16

Autosession functions ......................................................................6-17

Manipulating Auto Sessions ......................................................6-25

Chapter 7 Publisher .....................................................................................................7-1

Publisher ...........................................................................................7-3

To create a New Report .....................................................................7-3

Tools ...........................................................................................7-7

Report Tool Bar ..........................................................................7-8

Flexible Report by Sample ...........................................................7-9

Horizontal Table Report............................................................7-11

Intensity Report ........................................................................7-11

Method Detection Limit ...........................................................7-11

QC Trend Chart .......................................................................7-12

RSD Trend Chart ......................................................................7-13

Sample Report .................................................................................7-14

Simple Sample Report .....................................................................7-14

Trend Chart ....................................................................................7-15

Vertical Table Report .......................................................................7-15

Chapter 8 iTEVA Security ............................................................................................ 8-1

Introduction ......................................................................................8-1

Background .......................................................................................8-3

What is 21 CFR Part 11? ...........................................................8-3

Access Control ............................................................................8-3

User Login and Authentication ...................................................8-3

Electronic Records .......................................................................8-4

Electronic Signatures ..................................................................8-4

Audit Trails ..................................................................................8-4

Event Log ....................................................................................8-4

Access Control ..................................................................................8-5

Granting Access Rights ......................................................................8-7

Viewing the current User’s Access Rights ...........................................8-7

User Login and Authentication ...................................................8-8

iTEVA Security Login Process ......................................................8-8

Electronic Records .......................................................................8-9

Electronic Signatures ...................................................................8-9

Audit Trails ......................................................................................8-13

Event Logs ......................................................................................8-15

Information Events....................................................................8-16

Deleted Samples, Methods and Autosessions .............................8-16

Contents

Thermo Scientiﬁc iTEVA Software Manual v

Signing Samples and Sample Audit Trails ........................................8-17

Signing Methods and Method Audit Trail .......................................8-19

Signing Autosessions and Autosession Audit Trail ............................8-20

Contents

Thermo Scientiﬁc

vi

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Contents

Thermo Scientiﬁc iTEVA Software Manual vii

Figure 1-1. iTEVA login .............................................................1-5

Figure 1-2. iTEVA Security login ................................................1-5

Figure 2-1. e iTEVA Control Center window .........................2-3

Figure 2-2. e Menu Bar ..........................................................2-4

Figure 2-3. e File Menu ..........................................................2-4

Figure 2-4. Page Setup Dialog Box ..............................................2-5

Figure 2-5. View Menu ...............................................................2-6

Figure 2-6. Tools Menu ..............................................................2-6

Figure 2-7. Tools, Options, General ............................................2-7

Figure 2-8. Tools, Options, Periodic Table ..................................2-8

Figure 2-9. Tools, Options, Journal ............................................2-9

Figure 2-10. Tools, Options, Directories .....................................2-10

Figure 2-11. Tools, Options, Print Options ................................2-12

Figure 2-12. Tools, Options, Print Options, Header/Footer .......2-12

Figure 2-13. Tools, Options, Analyst ..........................................2-13

Figure 2-14. Tools, Options, New Method Parameters ...............2-14

Figure 2-15. Security Administration program, Access Control ...2-15

Figure 2-16. Tools, Options, Access Rights .................................2-16

Figure 2-17. Tools, Options, Application Database .....................2-18

Figure 2-18. iTEVA Database Wizard for standard (above)

and iTEVA Security (below) ........................2-19

Figure 2-19. Database Wizard .....................................................2-22

Figure 2-20. Database Wizard for iTEVA Security .......................2-22

Figure 2-21. Add a connection icon ............................................2-23

Figure 2-22. Data Link dialog box ..............................................2-23

Figure 2-23. Data link dialog box for iTEVA Security .................2-24

Figure 2-24. Data link le name dialog box ................................2-25

Figure 2-25. Change the Active Connection dropdown menu ....2-25

Figure 2-26. Edit/Add/Delete a connection icons .......................2-26

Figure 2-27. Database Upgrade dialog box ..................................2-26

Figure 2-28. Tools, Instrument Options, Autosampler ................2-27

Figure 2-29. Tools, Instrument Options, Sample Introduction ...2-27

Figure 2-30. e Help Menu ......................................................2-28

Figure 2-31. e Help Feature Request Incident Form ...............2-29

Figure 2-32. About iTEVA .........................................................2-30

Figure 2-33. e Tool Bar ...........................................................2-31

Figure 2-34. Journal window ......................................................2-32

Figure 2-35. Status Bar ...............................................................2-33

Figure 2-36. New Firmware Window..........................................2-34

Figures

Chapter 1

Chapter 2

Thermo Scientiﬁcviii iTEVA Software Manual

Figure 3-1. Analyst - Analysis, Method, Sequence .......................3-3

Figure 4-1. Method Menu Bar ....................................................4-3

Figure 4-2. Method Menu ..........................................................4-3

Figure 4-3. iCAP 6200 Method Template ...................................4-4

Figure 4-4. Method Workspace ...................................................4-5

Figure 4-5. Method, Periodic Table .............................................4-6

Figure 4-6. Method, Periodic Table, Cursor information for

specic element ........................................................4-6

Figure 4-7. Method, Periodic Table, Line List display .................4-7

Figure 4-8. Method, Periodic Table, Line List/Interferences

Window ...................................................................4-7

Figure 4-9. Method, Periodic Table, Selected element

displayed in aqua ..............................................4-8

Figure 4-10. Method, Periodic Table, Selected Line marked

with asterisk .....................................................4-8

Figure 4-11. Method, Status Window ...........................................4-9

Figure 4-12. Periodic Table, Map Editor .....................................4-10

Figure 4-13. Periodic Table, Right mouse click, Edit Map,

Add Lines .......................................................4-11

Figure 4-14. Periodic Table, Right mouse click, Add Lines,

Create .............................................................4-11

Figure 4-15. Method Workspace, Status .....................................4-12

Figure 4-16. Status Window .......................................................4-12

Figure 4-17. Method, Analysis Preferences ..................................4-13

Figure 4-18. Analysis Preferences ................................................4-13

Figure 4-19. Analysis Preferences, Sample Options .....................4-14

Figure 4-20. Analysis Preferences, Source ....................................4-15

Figure 4-21. Analysis Preferences, Maximum Integration Times .4-16

Figure 4-22. Analysis Preferences, Calibration Mode ..................4-16

Figure 4-23. Analysis Preferences, Trailing Fullframe Options .....4-18

Figure 4-24. Method, Automated Output ..................................4-20

Figure 4-25. Method, Automated Output dialog ........................4-21

Figure 4-26. Method, Automated Output, Standards .................4-23

Figure 4-27. Method, Automated Output, Standards .................4-23

Figure 4-28. Method, Report Preferences ....................................4-24

Figure 4-29. Report Preferences, Unknowns ...............................4-24

Figure 4-30. Report Preferences, Unknowns, Output and

Default View ...................................................4-25

Figure 4-31. Report Preferences, Unknowns,

In Concentration Output Mode, apply ...........4-25

Figure 4-32. Report Preferences, Unknowns, Calculate

Correction Factor. ..........................................4-26

Figure 4-33. Report Preferences, Unknowns, Screen Report, Print

Report and Exported Report ...........................4-27

Figure 4-34. Method, Checks .....................................................4-28

Figure 4-35. Checks Window .....................................................4-28

Figure 4-36. Checks, New Check Table Dialog Box ....................4-29

Figure 4-37. Checks Window .....................................................4-30

Chapter 3

Chapter 4

Figures

Thermo Scientiﬁc iTEVA Software Manual ix

Figure 4-38. Checks, QC Check Type ........................................4-31

Figure 4-39. Checks, Range Units ..............................................4-31

Figure 4-40. Checks, Standard Normalization type .....................4-32

Figure 4-41. Checks Window .....................................................4-33

Figure 4-42. Check Type, Recovery ............................................4-33

Figure 4-43. Check Type, Limit Check .......................................4-34

Figure 4-44. Check Type, Duplicate ...........................................4-35

Figure 4-45. e Method Workspace, Sequence Automation ......4-35

Figure 4-46. Sequence Automation .............................................4-36

Figure 4-47. Method, Sequence Automation, Initial Actions ......4-37

Figure 4-48. Method, Sequence Automation,

Continuing Actions ........................................4-38

Figure 4-49. Method, Sequence Automation, End Actions .........4-40

Figure 4-50. Method, Sequence Automation,

Global QC Properties .....................................4-41

Figure 4-51. Method, Sequence Automation,

Autosampler Options ......................................4-42

Figure 4-52. Method, Sequence Automation, Check table for

Intelligent Rinse ..............................................4-43

Figure 4-53. Method, Source Settings .........................................4-45

Figure 4-54. Method, Source Settings .........................................4-46

Figure 4-55. Method, Source Settings, Radial Viewing Height ..4-47

Figure 4-56. Method, Source Settings, Additional Gas Flow ......4-48

Figure 4-57. Method, Source Settings, Laser

Sample Introduction .......................................4-48

Figure 4-58. Method, Source Settings, SSEA

Sample Introduction .......................................4-50

Figure 4-59. Method, Internal Standards ....................................4-50

Figure 4-60. Method, Internal Standards, Periodic

Table Selection ................................................4-51

Figure 4-61. Method, Change Elements .....................................4-51

Figure 4-62. Method, Internal Standards Selection .....................4-52

Figure 4-63. Method, Standards .................................................4-53

Figure 4-64. Method, Standards Window ...................................4-54

Figure 4-65. Method, Standards, New Standard Dialog Box .......4-54

Figure 4-66. MSA Calibration ....................................................4-55

Figure 4-67. Method, Elements ..................................................4-56

Figure 4-68. Method, Elements ..................................................4-57

Figure 4-69. Method, Elements, General ....................................4-57

Figure 4-70. Elements, General, Result Labelling........................4-58

Figure 4-71. Method, Elements, General, Timing .......................4-58

Figure 4-72. Method, Elements, General, Referenced Internal ..........

Standards ........................................................4-59

Figure 4-73. Method, Elements, General, Analytical Report .......4-59

Figure 4-74. Method, Elements, Standards .................................4-61

Figure 4-75. Method, Elements, Standards table .........................4-62

Figure 4-76. Method, Elements, Standards, Re-Slope

Standards ........................................................4-62

Figure 4-77. Method, Elements, Fit ............................................4-63

Figures

Thermo Scientiﬁcx iTEVA Software Manual

Figure 4-78. Method, Elements, Fit, Line Switch and

Print Limits.....................................................4-65

Figure 4-79. Method, Elements, Standards, Line

Switching Arrows ............................................4-66

Figure 4-80. Method, Elements, Standards, Line

Switching for Ca .............................................4-66

Figure 4-81. Method, Setting Print Limits ..................................4-67

Figure 4-82. Use MSA- Blank subtraction ..................................4-68

Figure 4-83. Method, Element, Fit, Advanced Options ..............4-68

Figure 4-84. Method, Elements, Fit, Details ...............................4-70

Figure 4-85. Method, Elements, Fit, Std Table ............................4-72

Figure 4-86. Method, Elements, Fit, Right mouse click ..............4-73

Figure 4-87. Method, Elements, Fit, Calibration Plot

Commands, Print (Right mouse click) ............4-74

Figure 4-88. Method, Elements, IEC ..........................................4-75

Figure 4-89. Method, Elements, Subarray ...................................4-78

Figure 4-90. Right mouse click on Subarray Plot ........................4-79

Figure 4-91. Method, Method Reports .......................................4-80

Figure 4-92. Method, Method Reports, Common Report ..........4-80

Figure 4-93. Method, Open ........................................................4-81

Figure 4-94. Method Open, Select a Method Dialog Box ...........4-82

Figure 4-95. Method Query........................................................4-82

Figure 4-96. Method Query, Click Ellipsis ..................................4-83

Figure 4-97. Method Open, Select a Method Dialog Box -

Show All Revisions ..........................................4-83

Figure 4-98. Select a Method, Copy To, Select a Destination

Database dialog box ........................................4-84

Figure 4-99. Method Open, iTEVA Window after

Method is opened ...........................................4-84

Figure 4-100. Method Open, Select a Method Dialog Box for

iTEVA Security ................................................4-85

Figure 4-101. Method Open, Sign a Method Dialog Box

for iTEVA Security ........................................4-85

Figure 4-102. Method Open, Audit Trail for iTEVA Security .......4-86

Figure 4-103. Method, Close ........................................................4-86

Figure 4-104. Method, Save a Method Dialog Box .......................4-87

Figure 4-105. Method, Print Dialog Box ......................................4-88

Figure 4-106. Method Menu for iTEVA Security ..........................4-89

Figure 4-107. Method, Sign Method ............................................4-89

Figure 4-108. Method, Audit Trail ................................................4-90

Figure 4-109. Method, Tool Bar ...................................................4-90

Figure 4-110. Method Tool Bar ....................................................4-90

Figure 4-111. Tools Menu ............................................................4-92

Figure 4-112. Tools, Options, Change Element Display Order .....4-92

Figure 4-113. Tools, Options, New Method Parameters ...............4-93

Figures

Thermo Scientiﬁc iTEVA Software Manual xi

Figure 4-114. Help Menu .............................................................4-95

Figure 4-115. Help, About Analyst ...............................................4-95

Figure 5-1. Analysis Menu Bar ....................................................5-3

Figure 5-2. Method Tool Bar ......................................................5-3

Figure 5-3. View, Subarray Plot with multiple samples displayed 5-5

Figure 5-4. Method Menu ..........................................................5-6

Figure 5-5. Method Menu for iTEVA Security ............................5-7

Figure 5-6. Method, Sign Method ..............................................5-7

Figure 5-7. Method, Audit Trail ..................................................5-8

Figure 5-8. Run Menu ................................................................5-8

Figure 5-9. Run, Run Fullframe ..................................................5-9

Figure 5-10. Run, Run Fullframe, Sample ID Information ...........5-9

Figure 5-11. Run, Run Fullframe, Automated Output ................5-10

Figure 5-12. Run, Run Fullframe, Options .................................5-10

Figure 5-13. Low Wavelength Fullframe Image ...........................5-11

Figure 5-14. High Wavelength Fullframe Image .........................5-12

Figure 5-15. Fullframe Tool Bar ..................................................5-12

Figure 5-16. 2d Plot of Fullframe Image Region .........................5-14

Figure 5-17. Line Information ....................................................5-14

Figure 5-18. Analytical Element List ...........................................5-15

Figure 5-19. Line List for Elements in the Method .....................5-15

Figure 5-20. Fullframe Menu ......................................................5-15

Figure 5-21. Run, Run Time Scan ..............................................5-16

Figure 5-22. Run, Run Time Scan, Sample ID Information........5-16

Figure 5-23. Run, Run Time Scan, Automated Output ..............5-17

Figure 5-24. Run, Run Time Scan, Acquisition Parameters .........5-17

Figure 5-25. Run, Run Time Scan Options ................................5-18

Figure 5-26. Run, Run Time Scan, Select Lines ..........................5-18

Figure 5-27. Time Scan data being acquired ...............................5-19

Figure 5-28. Run, Time Scan, (Right mouse click) .....................5-20

Figure 5-29. Time Scan data shown as rst derivative .................5-21

Figure 5-30. Time Scan data with dened Gate values ................5-21

Figure 5-31. Run, Run Unknown ...............................................5-22

Figure 5-32. Run, Run Unknown, Sample ID Information ........5-22

Figure 5-33. Run, Run Unknown, Automated Output ...............5-23

Figure 5-34. Run, Run Unknown, Output mode: CONC ..........5-23

Figure 5-36. Run, Run Button ....................................................5-24

Figure 5-35. Run, Run Unknown, Preferences ............................5-24

Figure 5-37. MSA button ...........................................................5-25

Figure 5-38. Run, Select Lines Button ........................................5-25

Figure 5-39. Run, Run Unknown, Select Lines ..........................5-26

Figure 5-40. Run .......................................................................5-26

Figure 5-41. Run, Run Calibration .............................................5-27

Figure 5-42. Run, Calibration, Select Lines ................................5-29

Figure 5-43. Run, Start Continuous Run ....................................5-30

Figure 5-44. Method, Right mouse click .....................................5-31

Figure 5-45. Method Workspace, Right mouse click, Export All

Samples ...........................................................5-32

Figures

Chapter 5

Thermo Scientiﬁcxii iTEVA Software Manual

Figure 5-46. Method Workspace, Right mouse click,

Edit Report Option .......................................5-32

Figure 5-47. Method Workspace, Right mouse click menu

for iTEVA Security .........................................5-33

Figure 5-48. Method Workspace, Right mouse click,

Sign Method dialog box .................................5-33

Figure 5-49. Method Workspace, Right mouse click,

Method Audit Trail ........................................5-34

Figure 5-50. Method Workspace, Right mouse click

on samples .....................................................5-34

Figure 5-51. Method Workspace, Right mouse click,

Sample Identication .....................................5-35

Figure 5-52. Method Workspace, Right mouse click,

Recalculate Sample .........................................5-35

Figure 5-53. Method Workspace, Right mouse click,

Export Sample ................................................5-36

Figure 5-54. Method Workspace, Right mouse click,

Change Sample Type .....................................5-36

Figure 5-55. Method Workspace, Right mouse click menu

for iTEVA Security .........................................5-37

Figure 5-56. Method Workspace, Right mouse click,

Sign Sample ....................................................5-37

Figure 5-57. Method Workspace, Right mouse click,

Audit Trail .......................................................5-37

Figure 5-58. Method Workspace, Right mouse click

on Fullframe ...................................................5-38

Figure 5-59. Subtract Fullframe ..................................................5-39

Figure 5-60. Select the lename for subtraction ..........................5-39

Figure 5-61. Select lename for further subtraction ....................5-40

Figure 5-62. Resultant-2, Fullframe image ..................................5-40

Figure 5-63. Fullframe, Right mouse click,

Produce Sample dialog box .............................5-41

Figure 5-64. Fullframe, Right mouse click menu for

iTEVA Security ...............................................5-41

Figure 5-65. Fullframe, Right mouse click, Sign Sample .............5-42

Figure 5-66. Fullframe, Right mouse, Audit Trail ........................5-42

Figure 5-67. Results Menu ..........................................................5-43

Figure 5-68. Results, Typical Screen Report ................................5-43

Figure 5-69. Results, Print ..........................................................5-45

Figure 5-70. Results, Open .........................................................5-45

Figure 5-71. Results, Open, More button ...................................5-46

Figure 5-72. Results, Open, Sample Browser ..............................5-47

Figure 5-73. Results, Save ...........................................................5-47

Figure 5-74. Results, Export Results ...........................................5-48

Figure 5-75. Results, Open Sequence ..........................................5-49

Figure 5-76. Results, Delete Repeat ............................................5-49

Figure 5-77. Results, Run Recovery ............................................5-50

Figure 5-78. Results, Run Recovery, Analytical Report

- Recovery Check ............................................5-51

Figure 5-79. Results, Run Duplicate ...........................................5-51

Figures

Thermo Scientiﬁc iTEVA Software Manual xiii

Figure 5-80. Results, Run Duplicate, Analytical Report

- Duplicate Check ...........................................5-52

Figure 5-81. Select/Deselect Lines ..............................................5-52

Figure 5-82. Results, QC Actions ...............................................5-53

Figure 5-83. Results, QC Actions, Autocalc IECs .......................5-53

Figure 5-84. Calculated KI IEC factor displayed in Method,

Elements, IECs ..............................................5-54

Figure 5-85. Instrument Menu ...................................................5-54

Figure 5-86. Instrument, ICP Control Panel ...............................5-55

Figure 5-87. Instrument, ICP Control Panel and

Instrument Status ............................................5-55

Figure 5-88. Instrument, Perform Auto Peak ..............................5-57

Figure 5-89. Auto Peak Warning dialog box ................................5-58

Figure 5-90. Instrument, Torch Alignment .................................5-59

Figure 5-91. Instrument, Optimise Source ..................................5-59

Figure 5-92. Tools Menu ............................................................5-60

Figure 5-93. Tools, Example of a Wavelength Line Library .........5-61

Figure 5-94. Tools, Line Library, Right-click...............................5-62

Figure 5-96. Tools, Archive Fullframe Data ................................5-63

Figure 5-97. Tools, Archive Fullframe Data, Sample Browser ......5-64

Figure 5-98. Tools, Archive Fullframe Data, insert

media window ................................................5-64

Figure 5-99. Tools, Archive Fullframe Data, Select

Drive and Volume Label .................................5-65

Figure 5-100. Tools, Archive Fullframe Data, nish ......................5-65

Figure 5-101. Tools, Options ........................................................5-66

Figure 5-102. View Menu .............................................................5-67

Figure 5-103. View, Single Sample view ........................................5-67

Figure 5-104. View, Multiple Sample Presentation .......................5-68

Figure 5-105. Help, About Analyst ...............................................5-69

Figure 5-106. View, Subarray Plot with multiple

samples displayed ............................................5-70

Figure 6-1. Sequence Menu Bar ..................................................6-3

Figure 6-2. Auto-Session Menu...................................................6-4

Figure 6-3. Auto-Session, New Autosampler ...............................6-4

Figure 6-4. Auto-Session, New Autosampler dialog box ..............6-5

Figure 6-5. New Autosampler, New Sequence dialog box............6-5

Figure 6-6. Auto Session, New Autosampler dialog box ..............6-6

Figure 6-7. Auto-session Menu ...................................................6-7

Figure 6-9. Auto-Session, New Manual prompt ..........................6-8

Figure 6-8. Auto-Session, New Manual Dialog box ....................6-8

Figure 6-10. e iTEVA Window Sequence Tab .........................6-10

Figure 6-11. Sample List .............................................................6-11

Figure 6-12. Auto-Session menu for iTEVA Security ...................6-13

Figure 6-14. Auto-Session, Audit Trail ........................................6-14

Figure 6-13. Auto-Session, Sign ..................................................6-14

Figure 6-15. Sequence Menu ......................................................6-14

Chapter 6

Figures

Thermo Scientiﬁcxiv iTEVA Software Manual

Figure 6-16. Sequence, Add ........................................................6-15

Figure 6-17. Sequence, New Sequence ........................................6-15

Figure 6-18. Sequence, Remove ................................................6-16

Figure 6-19. e Sequence Tool Bar ...........................................6-16

Figure 6-20. Halt Auto-Session dialog box ..................................6-17

Figure 6-21. Assigning Sample Positions (Right mouse click) .....6-18

Figure 6-22. Auto-Locate Sample Positions .................................6-19

Figure 6-23. Unlocate, Right mouse click ...................................6-20

Figure 6-24. Sample U:1 position empty ....................................6-20

Figure 6-25. Sample relocated to position 42 ..............................6-21

Figure 6-26. Sample List showing relocation of

sample position 42. .........................................6-21

Figure 6-27. e Add Samples Dialog Box .................................6-22

Figure 6-28. Sample List .............................................................6-22

Figure 6-29. Sample List, Calculate Correction Factor ................6-23

Figure 6-30. Import Warning Dialog Box ...................................6-25

Figure 7-1. e Publisher Window .............................................7-3

Figure 7-2. Report/New le menu ..............................................7-3

Figure 7-3. Report/New dialog box .............................................7-4

Figure 7-4. Publisher, Sample Browser dialog box .......................7-4

Figure 7-5. Report Customization ..............................................7-5

Figure 7-6. Report Explorer ........................................................7-5

Figure 7-7. Report Menu ............................................................7-6

Figure 7-8. Export Options .......................................................7-6

Figure 7-9. Tools Menu ..............................................................7-7

Figure 7-10. Tool Bar....................................................................7-7

Figure 7-11. Report Customization Tab .......................................7-9

Figure 7-12. Method Data tab ...................................................7-10

Figure 7-13. Result Data Tab ......................................................7-10

Figure 7-14. Horizontal Table Report .........................................7-11

Figure 7-15. Intensity Report ......................................................7-11

Figure 7-16. Report Customization for MDL report ..................7-11

Figure 7-17. Method Detection Limit Report .............................7-12

Figure 7-18. QC Trend Chart .....................................................7-12

Figure 7-19. RSD Trend Chart ...................................................7-13

Figure 7-20. Sample Report ........................................................7-14

Figure 7-21. Simple Sample Report ............................................7-14

Figure 7-22. Trend Chart ............................................................7-15

Figure 7-23. Vertical Table Report ..............................................7-15

Figure 8-1. iTEVA Access Control Window ...............................8-5

Figure 8-2. iTEVA Access Rights Window ..................................8-7

Figure 8-3. New Users Window ................................................8-10

Figure 8-4. Default Signatures ..................................................8-10

Figure 8-5. Sign Sample Window .............................................8-12

Figure 8-6. Sign Method Window ............................................8-12

Chapter 7

Chapter 8

Figures

Thermo Scientiﬁc iTEVA Software Manual xv

Figures

Figure 8-7. Sign Autosession Window .....................................8-13

Figure 8-8. Audit Trail Window ................................................8-13

Figure 8-9. Event Viewer Window ............................................8-15

Figure 8-10. Event Properties Window .......................................8-15

Figure 8-11. Security Administration Window ...........................8-16

Figure 8-12. Sign Sample Window .............................................8-17

Figure 8-13. Sign Audit Trail Window ........................................8-18

Figure 8-14. Sign Method Window ............................................8-19

Figure 8-15. Sign Method, Audit Trail Window ..........................8-19

Figure 8-16. Auto-Session menu for iTEVA Security ...................8-20

Figure 8-17. Auto-Session, Sign ..................................................8-20

Figure 8-18. Auto-Session, Audit Trail ........................................8-21

Thermo Scientiﬁc

xvi

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Figures

Thermo Scientiﬁc iTEVA Software Manual 1 - 1

Chapter 1 Introduction

iTEVA is a powerful and exible Windows®- based application that is

used to acquire, process, store and report analytical data from ermo

Scientic’s iCAP ICP spectrometers.

is manual describes the features of the program and explains how

the analyst can generate analytical methods and data processing

routines to determine the concentration of elements in complex

samples. e program includes a broad variety of features to allow the

analyst to congure methods and sequences to obtain manual and

automated analytical results.

Thermo Scientiﬁc1 - 2 iTEVA Software Manual

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Introduction

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Thermo Fisher Scientific iTEVA Software Owner's manual

Thermo Fisher Scientific iTEVA Software Owner's manual

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