Taylor Technologies K-1548 Owner's manual

Type
Owner's manual
InstructionNumber:5401
Component Description
> DROPTEST
>SULFURICACID(Sulfuric,Phosphoric,orSulfamicAcid)
> (1drop=1g/100mL)
COMPONENTS:
1x4029 Pipet,Calibrated0.5&1.0mL,plastic
1x5401 Instruction
1x9198 SampleTube,Graduated,25mL,plastic
w/cap
1xR‐0645TotalAlkalinityIndicator,DB
1xR‐0740SodiumHydroxideReagent,DB
TOORDERREPLACEMENTPARTSANDREAGENTSCALLTOLL‐FREE
800‐TESTKIT(800‐837‐8548).
PROCEDURE:
CAREFULLYREADANDFOLLOWPRECAUTIONSONREAGENT
LABELS.KEEPREAGENTSAWAYFROMCHILDREN.
1. Usinga1.0mLpipet(#4029),add0.5mLacid
solutiontobetestedto25mLsampletube(#9198).
NOTE:Forphosphoricorsulfamicacid,add1.0mLacid
solutiontobetestedto25mLsampletube.
2. Dilutetoapproximately1/3fullwithtapwater.
3. Add5dropsR‐0645TotalAlkalinityIndicator.
Swirltomix.Sampleshouldturnred.
4. AddR‐0740SodiumHydroxideReagentdropwise,
swirlingandcountingaftereachdrop,untilcolor
changesfromredtogreen.Alwaysholdbottlein
verticalposition.
5. RecorddropsofR‐0740SodiumHydroxideReagentas
gramsper100mL(g/100mL),whichisalmostthe
sameaspercent.
NOTE:Athigherconcentrationsofsulfuricand
phosphoricacid,thedifferencebetweengrams
perhundredmillilitersandpercentcanbe
considerable.Consultthefollowingtablesfor
correctionstobeapplied.(Sulfamicacidisa
solidnotlikelytobeabove15%insolution.)
SULFURICACID(H2SO4)
gramsper100mL percent
10 9.4
20 17.8
30 25.4
40 32.3
50 38.7
60 44.6
70 50.1
80 55.25
90 60.0
100 64.6
110 68.9
120 74.0
Instructions
130 76.9
140 80.7
150 84.5
160 89.6
170 93.0
180 99.0
PHOSPHORICACID(H3PO4)
gramsper100mL percent
10 9.5
20 18.0
30 26.0
40 33.2
50 39.9
60 46.1
70 51.8
80 57.1
90 62.1
100 66.9
110 71.4
120 75.7
130 79.8
140 83.6
150 87.4
160 91.0
170 94.5
180 97.8
187 100.0
SULFURICACID(H2SO4)
NOTE:Dropequivalencecanbechangedbyadjustingthe
samplesizeinStep1.Instrongacidsolutions
(above1%)dilutioncanbemadebyusingtap
water.Inweakeracidsolutions,deionizedor
distilledwatershouldbeusedfordilution.
Sample DropEquivalencefor
SizeUsed SulfuricAcid
0.5mL 1dr=1.0g/100mL(%)
1.0mL 1dr=0.5g/100mL(%)
10.0mL 1dr=0.05g/100mL(500ppm)
20.0mL 1dr=0.025g/100mL(250ppm)
25.0mL 1dr=0.02g/100mL(200ppm)
DropEquivalencefor
Sample PhosphoricAcid
SizedUsed orSulfamicAcid
0.5mL 1dr=2.0g/100mL(%)
1.0mL 1dr=1.0g/100mL(%)
10.0mL 1dr=0.1g/100mL(1000ppm)
20.0mL 1dr=0.05g/100mL(500ppm)
25.0mL 1dr=0.04g/100mL(400ppm)
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Taylor Technologies K-1548 Owner's manual

Type
Owner's manual

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