Rosemount 3500P/3500VP PERpH-X High Performance pH/ORP Sensors Quick start guide

Type
Quick start guide

The Rosemount 3500P/3500VP PERpH-X High Performance pH/ORP Sensors offer reliable and accurate pH and ORP measurement in various industrial applications. With a variety of sensor designs, including submersible, insertion, and retractable, these sensors can meet the demands of different process conditions. The sensors feature a preamplifier that amplifies the signal near the measurement point, ensuring a strong signal-to-noise ratio and immunity to electrical interference. They also have a built-in reference electrode with a long service life, reducing maintenance requirements.

The Rosemount 3500P/3500VP PERpH-X High Performance pH/ORP Sensors offer reliable and accurate pH and ORP measurement in various industrial applications. With a variety of sensor designs, including submersible, insertion, and retractable, these sensors can meet the demands of different process conditions. The sensors feature a preamplifier that amplifies the signal near the measurement point, ensuring a strong signal-to-noise ratio and immunity to electrical interference. They also have a built-in reference electrode with a long service life, reducing maintenance requirements.

Quick Start Guide
00825-0200-3300, Rev AA
November 2020
Rosemount 3500P/3500VP
PERpH-X High Performance pH/ORP
Sensors
Essential instructions
Read this page before proceeding!
Emerson designs, manufactures, and tests its products to meet many national and international
standards. Because these instruments are sophisticated technical products, you must properly install,
use, and maintain them to ensure they continue to operate within their normal specifications. You
must adhere to the following instructions and integrate them into your safety program when
installing, using, and maintaining Emerson's Rosemount
products. Failure to follow the proper
instructions may cause any one of the following situations to occur: loss of life, personal injury,
property damage, damage to this instrument, and warranty invalidation.
Read all instructions prior to installing, operating, and servicing the product.
If you do not understand any of the instructions, contact your Emerson representative for
clarification.
Follow all warnings, cautions, and instructions marked on and supplied with the product.
Inform and educate your personnel in the proper installation, operation, and maintenance of the
product.
Install equipment as specified in the installation instructions of the appropriate Quick Start Guide
and per applicable local and national codes. Connect all products to the proper electrical and
pressure sources.
To ensure proper performance, use qualified personnel to install, operate, update, program, and
maintain the product.
When replacement parts are required, ensure that qualified people use replacement parts
specified by Emerson. Unauthorized parts and procedures can affect the product's performance,
place the safe operation of your process at risk, and may result in fire, electrical hazards, or
improper operation.
Ensure that all equipment doors are closed and protective covers are in place, except when
maintenance is being performed by qualified people, to prevent electrical shock and personal
injury.
Note
The information contained in this document is subject to change without notice.
WARNING
Pressure and temperature
Before removing the sensor, be absolutely certain that the process pressure is reduced to 0 psig
and the process temperature is lowered to a safe level.
Do not insert or retract retractable sensors when process pressures are in excess of 64 psig (542
kPa) for option 21 or 35 psig (343 kPa) for option 25.
WARNING
Physical access
Unauthorized personnel may potentially cause significant damage to and/or misconfiguration of end
users’ equipment. This could be intentional or unintentional and needs to be protected against.
Physical security is an important part of any security program and fundamental to protecting your
system. Restrict physical access by unauthorized personnel to protect end users’ assets. This is true for
all systems used within the facility.
Quick Start Guide November 2020
2 Emerson.com/Rosemount
CAUTION
Sensor/process application compatibility
The wetted sensor materials may not be compatible with process composition and operating
conditions.
Application compatibility is entirely the operator's responsibility.
Contents
Install........................................................................................................................................... 5
Start up and calibrate................................................................................................................. 16
Maintenance.............................................................................................................................. 18
Rosemount pH/ORP sensor(s) product certifications..................................................................20
Declaration of Conformity..........................................................................................................27
China RoHS table........................................................................................................................29
Intrinsically safe sensor installation drawing - FM........................................................................30
November 2020 Quick Start Guide
Quick Start Guide 3
Quick Start Guide November 2020
4 Emerson.com/Rosemount
1 Install
1.1 Storage
1. Emerson recommends storing electrodes in their original shipping
containers until needed.
2. Store electrodes with a protective cap containing KCl solution
(PN 9210342).
3. For overnight storage, immerse the sensor in tap water or 4 pH
buffer solution.
1.2 Installation
Figure 1-1: Rosemount 3500P and 3500VP Sensor Dimensional Drawing
November 2020 Quick Start Guide
Quick Start Guide 5
Figure 1-2: Jet Spray Cleaner
A. Cleaning solution by others
B. Solenoid valve or manual valve (supplied by others)
C. Corrosion resistant tubing (supplied by others)
D. Polypropylene ¼-in. compression fitting
E. ¼-in. 316 stainless steel
F. ¼-in. polypropylene
G. Stainless set screw for adjustable spray nozzle height
H. 2-in. NPT threads
I. Sensor
J. 1-in. PVC coupling for submersible applications (supplied by others)
K. 1-in. PVC or stainless conduit (supplied by others)
L. Cable
M. Timer supplied by others or use timer feature in Rosemount instrument
Quick Start Guide November 2020
6 Emerson.com/Rosemount
Figure 1-3: Rosemount 3500P and 3500VP Flow through Installation
A. 1½-in. (38.1 mm) schedule 80 CPVC tee with 1-in. (25.4 mm) female
national pipe thread (FNPT) connections (code 16) straight flow shown
B. Always mount sensor at least 10 degrees above horizontal.
C. 1½-in. (38.1 mm) pipe "Y"
D. 1½-in. x 1-in. (38.1 x 25.4 mm) reducing bushing
E. Flow
F. 1½-in. (38.1 mm) schedule 80 CPVC with view or cleaning port
G. Angle flow shown
November 2020 Quick Start Guide
Quick Start Guide 7
Figure 1-4: Submersion Installation: Handrail Mounting Accessory (PN
11275-01)
A. Sensor cable
B. 1½-in. (38.1 mm) PVC pipe schedule 80
C. 1½-in. (38.1 mm) pipe clamp, three places
D. 45-degree sweep ell extension pipe
E. Regularly check to make sure connections are water tight
F. Unistrut 1-in. x 1-in. (41.3 x 41. 3 mm) aluminum
G. 1½-in. (38.1 mm) pipe clamp, two places
H. Can be any convenient dimension
I. Customer handrail, two places
J. Mounting channel aluminum, two places
K. Locking pin with bead chain
Note
Unless otherwise specified.
Quick Start Guide November 2020
8 Emerson.com/Rosemount
1.3 Wiring
For additional wiring information on this product, including sensor
combinations not shown here, please refer to Emerson.com/
RosemountLiquidAnalysisWiring.
Figure 1-5: Rosemount PERpH-X Sensors, Preamplifier in Analyzer
For Rosemount 3500P and 3500VP, option codes -02, -07, and -08
Non-preamplifier sensors
Blue cable
Table 1-1: Rosemount PERpH-X Sensors, Preamplifier in Analyzer
Wire color Rosemount 56, 1056,
1057, and 1066 terminal
number
Rosemount 54e and 5081
terminal number
Rosemount
XMT terminal
number
N/A Inner drain (no
connection)
N/A N/A
N/A N/A 1 N/A
Green Connect to instrument
ground or as shown
2 N/A
White Resistance temperature
device (RTD) return
3 1
White/red RTD sense 4 2
Red RTD in 5 3
White/gray Reference shield 6 4
Gray Reference in 7 5
Blue Solution ground 8 6
Clear mV/pH shield 9 7
November 2020 Quick Start Guide
Quick Start Guide 9
Table 1-1: Rosemount PERpH-X Sensors, Preamplifier in Analyzer (continued)
Wire color Rosemount 56, 1056,
1057, and 1066 terminal
number
Rosemount 54e and 5081
terminal number
Rosemount
XMT terminal
number
Orange mV/pH in 10 8
N/A -5 Vdc 11 9
N/A +5 Vdc 12 10
Quick Start Guide November 2020
10 Emerson.com/Rosemount
Figure 1-6: Rosemount PERpH-X Sensors, Preamplifier in Junction Box
For Rosemount 3500P and 3500VP, option codes -02, -07, and -08
Non-preamplifier sensors
Blue cable
Extension cable PN 23646-01 or 9200273 shown.
Can also use extension cable PN 9200348; extend color scheme from sensor
or VP8 cable instead of using shown wiring scheme.
Table 1-2: Rosemount PERpH-X Sensors, Preamplifier in Junction Box
Wire
color
Junction
box
terminal
number
Extension
cable
color
Rosemount 56,
1056, 1057, and
1066 terminal
number
Rosemount 54e
and 5081
terminal
number
Rosemount
XMT terminal
number
N/A N/A N/A Inner drain (no
connection)
N/A N/A
N/A 1 N/A N/A 1 N/A
Green 2 Inner drain Connect to
instrument
ground as shown
2 N/A
White 3 White RTD return 3 1
White/red 4 White/red RTD sense 4 2
Red 5 Red RTD in 5 3
White/
gray
6 White/
gray
Reference shield 6 4
Gray 7 Gray Reference in 7 5
Blue 8 Blue Solution ground 8 6
November 2020 Quick Start Guide
Quick Start Guide 11
Table 1-2: Rosemount PERpH-X Sensors, Preamplifier in Junction Box (continued)
Wire
color
Junction
box
terminal
number
Extension
cable
color
Rosemount 56,
1056, 1057, and
1066 terminal
number
Rosemount 54e
and 5081
terminal
number
Rosemount
XMT terminal
number
Clear 9 White/
black
mV/pH shield 9 7
Orange 10 Black mV/pH in 10 8
N/A 11 Brown -5 Vdc 11 9
N/A 12 Green +5 Vdc 12 10
Quick Start Guide November 2020
12 Emerson.com/Rosemount
Figure 1-7: PERpH-X Sensors, Preamplifier in Sensor
For Rosemount 3500P and 3500VP, option codes -01, -03, -04, -05, and -06
Preamplifier in sensor
Blue cable
Table 1-3: Rosemount PERpH-X Sensors, Preamplifier in Sensor
Wire color Rosemount 56,
1056, 1057, and
1066 terminal
number
Rosemount 54e and
5081 terminal
number
Rosemount XMT
terminal number
N/A N/A 1 N/A
Green Connect to
instrument ground or
as shown
2 N/A
White RTD return 3 1
White/ red RTD sense 4 2
Red RTD in 5 3
N/A Reference shield 6 4
Gray Reference in 7 5
Blue Solution ground 8 6
Clear mV/pH shield 9 7
Orange mV/pH in 10 8
White/gray -5 Vdc 11 9
Inner drain +5 Vdc 12 10
November 2020 Quick Start Guide
Quick Start Guide 13
Figure 1-8: Rosemount PERpH-X Sensors, Preamplifier in Sensor,
Junction Box Used for Extending Cable
For Rosemount 3500P and 3500VP, option codes -01, -03, -04, -05, and -06
Preamplifier in sensor
Blue cable
Extension cable PN 23646-01 or 9200273 shown.
Can also use extension cable PN 9200348: white/gray is replacement wire
color for brown wire.
Table 1-4: Rosemount PERpH-X Sensors, Preamplifier in Sensor, Junction Box
Used for Extending Cable
Wire
color
Junction
box
terminal
number
Extension
cable color
Rosemount 56,
1056, 1057,
and 1066
terminal
number
Rosemount
54e and 5081
terminal
number
Rosemount
XMT terminal
number
N/A 1 N/A N/A 1 N/A
Green 2 Inner drain.
Connect to
instrument
ground or as
shown.
N/A 2 N/A
White 3 White RTD return 3 1
White/re
d
4 White/red RTD sense 4 2
Red 5 Red RTD in 5 3
N/A 6 White/gray (no
connection)
Reference
shield
6 4
Gray 7 Gray Reference in 7 5
Quick Start Guide November 2020
14 Emerson.com/Rosemount
Table 1-4: Rosemount PERpH-X Sensors, Preamplifier in Sensor, Junction Box
Used for Extending Cable (continued)
Wire
color
Junction
box
terminal
number
Extension
cable color
Rosemount 56,
1056, 1057,
and 1066
terminal
number
Rosemount
54e and 5081
terminal
number
Rosemount
XMT terminal
number
Blue 8 Blue Solution ground 8 6
Clear
(orange
shield)
9 White/black pH shield 9 7
Orange 10 Black pH in 10 8
White/
gray
11 Brown -5 Vdc 11 9
ID (inner
drain)
12 Green +5 Vdc 12 10
November 2020 Quick Start Guide
Quick Start Guide 15
2 Start up and calibrate
2.1 Prepare electrode
Procedure
1. Remove electrode from shipping container.
2. Remove the protective boot covering the electrode bulb.
3. Rinse away salt film with clean water; then shake the electrode so
that the internal solution fills the bulb, thus removing any air trapped
there.
2.2 Calibrate with two point pH buffer solution
Select two stable buffer solutions, preferably pH 4.0 and pH 7.0. You can use
buffers other than pH 4.0 and pH 7.0 as long as the pH values are least two
pH units apart.
Note
A pH 7 buffer solution reads an mV value of approximately zero, and pH
buffers read approximately ±59.1 mV for each pH unit above or below pH 7.
Check the pH buffer manufacturer specifications for milivolt values at
various temperatures, since temperature may affect the actual value of the
pH buffer solution mV/pH value.
Procedure
1. Immerse the sensor in buffer solution.
Make sure the buffer solution contacts the metal housing of the
sensor, which acts as the solution ground contact.
2. Allow sensor to equilibrate to the buffer temperature and wait for the
reading to stabilize.
The transmitter can now acknowledge the value of the buffer.
3. Rinse the buffer solution off of the sensor with distilled or deionized
water.
4. Repeat steps Step 1 through Step 3 using the second buffer solution.
The theoretical slope value, according to the Nernst equation for calculating
pH, is approximately 59.17 mV/pH. Over time the sensor will age, both in
the process and in storage, and this will result in reduced slope values. To
ensure accurate readings, Emerson recommends replacing the electrode
when the slope value falls below 47 to 49 mV/pH.
2.3
Standardize pH sensor
For maximum accuracy, you can standardize the sensor in-line or with a
process grab sample after performing a buffer calibration and conditioning
Quick Start Guide November 2020
16 Emerson.com/Rosemount
the sensor to the process. Standardization accounts for the sensor junction
potential and other interferences. Standardization does not change the
sensor's slope, but simply adjusts the transmitter's reading to match that of
a known process pH.
November 2020 Quick Start Guide
Quick Start Guide 17
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Rosemount 3500P/3500VP PERpH-X High Performance pH/ORP Sensors Quick start guide

Type
Quick start guide

The Rosemount 3500P/3500VP PERpH-X High Performance pH/ORP Sensors offer reliable and accurate pH and ORP measurement in various industrial applications. With a variety of sensor designs, including submersible, insertion, and retractable, these sensors can meet the demands of different process conditions. The sensors feature a preamplifier that amplifies the signal near the measurement point, ensuring a strong signal-to-noise ratio and immunity to electrical interference. They also have a built-in reference electrode with a long service life, reducing maintenance requirements.

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